1-N-[(S)-4-benzyloxycarbonylamino-2-benzyloxybutylyl]-2-benzyloxy-3,2′,6′-tris(N-benzyloxycarbonyl)-3′,4′-dideoxyneamine

Base Information

Chemical Name:1-N-[(S)-4-benzyloxycarbonylamino-2-benzyloxybutylyl]-2-benzyloxy-3,2′,6′-tris(N-benzyloxycarbonyl)-3′,4′-dideoxyneamine
CAS No.:959918-82-2
Molecular Formula:C₆₂H₆₉N₅O₁₅
Molecular Weight:1124.25
Hs Code.:

Synonyms:1-N-[(S)-4-benzyloxycarbonylamino-2-benzyloxybutylyl]-2-benzyloxy-3,2′,6′-tris(N-benzyloxycarbonyl)-3′,4′-dideoxyneamine

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Chemical Property of 1-N-[(S)-4-benzyloxycarbonylamino-2-benzyloxybutylyl]-2-benzyloxy-3,2′,6′-tris(N-benzyloxycarbonyl)-3′,4′-dideoxyneamine

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Technology Process of 1-N-[(S)-4-benzyloxycarbonylamino-2-benzyloxybutylyl]-2-benzyloxy-3,2′,6′-tris(N-benzyloxycarbonyl)-3′,4′-dideoxyneamine

There total 2 articles about 1-N-[(S)-4-benzyloxycarbonylamino-2-benzyloxybutylyl]-2-benzyloxy-3,2′,6′-tris(N-benzyloxycarbonyl)-3′,4′-dideoxyneamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₂₃H₂₄N₂O₇

: 959918-81-1
2-benzyloxy-3,2',6'-tri-N-benzyloxycarbonyl-3',4'-dideoxyneamine

: 959918-82-2
1-N-[(S)-4-benzyloxycarbonylamino-2-benzyloxybutylyl]-2-benzyloxy-3,2′,6′-tris(N-benzyloxycarbonyl)-3′,4′-dideoxyneamine

Guidance literature:: With triethylamine; In tetrahydrofuran; at 50 - 53 ℃; for 3.5 - 4.5h; Product distribution / selectivity;

Reference yield:

: 959918-79-7
2-benzyloxy-1,3,2',6'-tetra-N-benzyloxycarbonyl-3',4'-dideoxyneamine

: 959918-82-2
1-N-[(S)-4-benzyloxycarbonylamino-2-benzyloxybutylyl]-2-benzyloxy-3,2′,6′-tris(N-benzyloxycarbonyl)-3′,4′-dideoxyneamine

Guidance literature:: Multi-step reaction with 2 steps

1: sodium hydride / N,N-dimethyl-formamide / 20 °C

2: sodium hydride / water; 1,4-dioxane / 80 °C

With sodium hydride; In 1,4-dioxane; water; N,N-dimethyl-formamide;
DOI:10.1038/ja.2017.60