1-O-Acetyl-2-desoxy-3,4-O-isopropyliden-2-nitro-6-O-trityl-β-D-psicofuranose

Base Information

• Chemical Name: 1-O-Acetyl-2-desoxy-3,4-O-isopropyliden-2-nitro-6-O-trityl-β-D-psicofuranose
• CAS No.: 85398-13-6
• Molecular Formula: C₃₀H₃₁NO₈
• Molecular Weight: 533.578

Synonyms:1-O-Acetyl-2-desoxy-3,4-O-isopropyliden-2-nitro-6-O-trityl-β-D-psicofuranose

Chemical Property of 1-O-Acetyl-2-desoxy-3,4-O-isopropyliden-2-nitro-6-O-trityl-β-D-psicofuranose

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 1-O-Acetyl-2-desoxy-3,4-O-isopropyliden-2-nitro-6-O-trityl-β-D-psicofuranose

There total 2 articles about 1-O-Acetyl-2-desoxy-3,4-O-isopropyliden-2-nitro-6-O-trityl-β-D-psicofuranose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

acetic anhydride (108-24-7) + 2-Desoxy-3,4-O-isopropyliden-2-nitro-6-O-trityl-β-D-psicofuranose → 1-O-Acetyl-2-desoxy-3,4-O-isopropyliden-2-nitro-6-O-trityl-β-D-psicofuranose (85398-13-6)

Guidance literature:

With pyridine; for 1h; Ambient temperature;

DOI:10.1002/hlca.19820650730

Reference yield:

1-Desoxy-1-nitro-2,3-O-isopropyliden-5-O-trityl-D-ribofuranose → 1-O-Acetyl-2-desoxy-3,4-O-isopropyliden-2-nitro-6-O-trityl-β-D-psicofuranose (85398-13-6)

Guidance literature:

Multi-step reaction with 2 steps

1: K₂CO₃ / methanol / 2.33 h / Ambient temperature

2: 92 percent / pyridine / 1 h / Ambient temperature

With pyridine; potassium carbonate; In methanol;

DOI:10.1002/hlca.19820650730

Reference yield: 87.0%

1-O-Acetyl-2-desoxy-3,4-O-isopropyliden-2-nitro-6-O-trityl-β-D-psicofuranose (85398-13-6) → Acetic acid (3aS,6R,6aR)-2,2-dimethyl-6-trityloxymethyl-tetrahydro-furo[3,4-d][1,3]dioxol-4-ylmethyl ester

Guidance literature:

With 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; In benzene; for 8h; Heating;

DOI:10.1002/hlca.19830660733

upstream raw materials:

acetic anhydride

Downstream raw materials:

1-O-acetyl-2,6-anhydro-3,4-O-isopropylidene-β-D-psicofuranose

1-(1-O-acetyl-3,4-O-isopropylidene-6-O-trityl-D-psicofuranosyl)uracil

Post a RFQ

Cas No.:

Product Name:

Quantity:

Please select Metric Ton KG G Pound L ML

Email:

Company name:

Valid Period:

Detailed Requirements:

• Sample
• MOQ
• GMP
• FDA
• Price
  FOB CIF CFR EXW
• Urgent purchase

Enter 15 to 2000 letters.Word count: 0 letters

Attach files(File Format: Jpeg, Jpg, Gif, Png, PDF, PPT, Zip, Rar,Word or Excel Maximum File Size: 3MB)

Remove

Submit

1

What can I do for you?
Get Best Price

Get Best Price for 85398-13-6 1-O-Acetyl-2-desoxy-3,4-O-isopropyliden-2-nitro-6-O-trityl-β-D-psicofuranose

Send

Send

Metric Ton KG G Pound L ML

Send

Send