Technology Process of C32H30F3N3O7
There total 5 articles about C32H30F3N3O7 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
water; trifluoroacetic acid;
In
dichloromethane;
at 20 ℃;
for 3h;
DOI:10.1002/anie.201404158
- Guidance literature:
-
Multi-step reaction with 5 steps
1: perchloric acid / 12 h / 20 °C
2: O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / dichloromethane / 2 h / 20 °C
3: piperidine / N,N-dimethyl-formamide / 2 h / 20 °C
4: N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 12 h / 20 °C
5: water; trifluoroacetic acid / dichloromethane / 3 h / 20 °C
With
piperidine; perchloric acid; water; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid;
In
dichloromethane; N,N-dimethyl-formamide;
DOI:10.1002/anie.201404158
- Guidance literature:
-
Multi-step reaction with 4 steps
1: O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / dichloromethane / 2 h / 20 °C
2: piperidine / N,N-dimethyl-formamide / 2 h / 20 °C
3: N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 12 h / 20 °C
4: water; trifluoroacetic acid / dichloromethane / 3 h / 20 °C
With
piperidine; water; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid;
In
dichloromethane; N,N-dimethyl-formamide;
DOI:10.1002/anie.201404158