(2S,3R,4S,6R)-4-(dimethylamino)-2-((1R,3R,6R,8R,9R,10R,12R,13S,17S)-3-ethyl-10-methoxy-6,8,10,12,15,15,17-heptamethyl-2-methylene-5,7-dioxo-4,14,16-trioxabicyclo[11.3.1]heptadecan-9-yloxy)-6-methyltetrahydro-2H-pyran-3-yl benzoate

Base Information

• Chemical Name: (2S,3R,4S,6R)-4-(dimethylamino)-2-((1R,3R,6R,8R,9R,10R,12R,13S,17S)-3-ethyl-10-methoxy-6,8,10,12,15,15,17-heptamethyl-2-methylene-5,7-dioxo-4,14,16-trioxabicyclo[11.3.1]heptadecan-9-yloxy)-6-methyltetrahydro-2H-pyran-3-yl benzoate
• CAS No.: 1261067-65-5
• Molecular Formula: C₄₀H₆₁NO₁₀
• Molecular Weight: 715.925

Synonyms:(2S,3R,4S,6R)-4-(dimethylamino)-2-((1R,3R,6R,8R,9R,10R,12R,13S,17S)-3-ethyl-10-methoxy-6,8,10,12,15,15,17-heptamethyl-2-methylene-5,7-dioxo-4,14,16-trioxabicyclo[11.3.1]heptadecan-9-yloxy)-6-methyltetrahydro-2H-pyran-3-yl benzoate

Chemical Property of (2S,3R,4S,6R)-4-(dimethylamino)-2-((1R,3R,6R,8R,9R,10R,12R,13S,17S)-3-ethyl-10-methoxy-6,8,10,12,15,15,17-heptamethyl-2-methylene-5,7-dioxo-4,14,16-trioxabicyclo[11.3.1]heptadecan-9-yloxy)-6-methyltetrahydro-2H-pyran-3-yl benzoate

Chemical Property:

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Technology Process of (2S,3R,4S,6R)-4-(dimethylamino)-2-((1R,3R,6R,8R,9R,10R,12R,13S,17S)-3-ethyl-10-methoxy-6,8,10,12,15,15,17-heptamethyl-2-methylene-5,7-dioxo-4,14,16-trioxabicyclo[11.3.1]heptadecan-9-yloxy)-6-methyltetrahydro-2H-pyran-3-yl benzoate

There total 1 articles about (2S,3R,4S,6R)-4-(dimethylamino)-2-((1R,3R,6R,8R,9R,10R,12R,13S,17S)-3-ethyl-10-methoxy-6,8,10,12,15,15,17-heptamethyl-2-methylene-5,7-dioxo-4,14,16-trioxabicyclo[11.3.1]heptadecan-9-yloxy)-6-methyltetrahydro-2H-pyran-3-yl benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.6%

(2S,3R,4S,6R)-4-(dimethylamino)-2-((1R,3R,6R,7S,8S,9R,10R,12R,13S,17S)-3-ethyl-7-hydroxy-10-methoxy-6,8,10,12,15,15,17-heptamethyl-2-methylene-5-oxo-4,14,16-trioxabicyclo[11.3.1]heptadecan-9-yloxy)-6-methyltetrahydro-2H-pyran-3-yl benzoate (1111873-45-0) → (2S,3R,4S,6R)-4-(dimethylamino)-2-((1R,3R,6R,8R,9R,10R,12R,13S,17S)-3-ethyl-10-methoxy-6,8,10,12,15,15,17-heptamethyl-2-methylene-5,7-dioxo-4,14,16-trioxabicyclo[11.3.1]heptadecan-9-yloxy)-6-methyltetrahydro-2H-pyran-3-yl benzoate (1261067-65-5)

Guidance literature:

With Dess-Martin periodane; In dichloromethane; at 20 ℃; for 1h;

DOI:10.1016/j.ejmech.2010.09.060

Reference yield: 98.2%

Diazoethan (1117-96-0) + (2S,3R,4S,6R)-4-(dimethylamino)-2-((1R,3R,6R,8R,9R,10R,12R,13S,17S)-3-ethyl-10-methoxy-6,8,10,12,15,15,17-heptamethyl-2-methylene-5,7-dioxo-4,14,16-trioxabicyclo[11.3.1]heptadecan-9-yloxy)-6-methyltetrahydro-2H-pyran-3-yl benzoate (1261067-65-5) → (2S,3R,4S,6R)-4-(dimethylamino)-2-((1R,3R,6R,8R,9R,10R,12R,13S,17S)-3-ethyl-10-methoxy-3',6,8,10,12,15,15,17-octamethyl-5,7-dioxo-3',5'-dihydro-4,14,16-trioxaspiro[bicyclo[11.3.1]heptadecane-2,4'-pyrazole]-9-yloxy)-6-methyltetrahydro-2H-pyran-3-yl benzoate (1261067-71-3)

Guidance literature:

In diethyl ether; at 0 - 25 ℃; for 49h; Darkness;

DOI:10.1016/j.ejmech.2010.09.060

Reference yield: 89.0%

diazomethane (186581-53-3,908094-01-9,334-88-3) + (2S,3R,4S,6R)-4-(dimethylamino)-2-((1R,3R,6R,8R,9R,10R,12R,13S,17S)-3-ethyl-10-methoxy-6,8,10,12,15,15,17-heptamethyl-2-methylene-5,7-dioxo-4,14,16-trioxabicyclo[11.3.1]heptadecan-9-yloxy)-6-methyltetrahydro-2H-pyran-3-yl benzoate (1261067-65-5) → (2S,3R,4S,6R)-4-(dimethylamino)-2-((1R,3R,6R,8R,9R,10R,12R,13S,17S)-3-ethyl-10-methoxy-6,8,10,12,15,15,17-heptamethyl-5,7-dioxo-3',5'-dihydro-4,14,16-trioxaspiro[bicyclo[11.3.1]heptadecane-2,4'-pyrazole]-9-yloxy)-6-methyltetrahydro-2H-pyran-3-yl benzoate (1111873-50-7)

Guidance literature:

In diethyl ether; at 0 - 25 ℃; for 49h; Darkness;

DOI:10.1016/j.ejmech.2010.09.060

upstream raw materials:

(2S,3R,4S,6R)-4-(dimethylamino)-2-((1R,3R,6R,7S,8S,9R,10R,12R,13S,17S)-3-ethyl-7-hydroxy-10-methoxy-6,8,10,12,15,15,17-heptamethyl-2-methylene-5-oxo-4,14,16-trioxabicyclo[11.3.1]heptadecan-9-yloxy)-6-methyltetrahydro-2H-pyran-3-yl benzoate

Downstream raw materials:

(2S,3R,4S,6R)-4-(dimethylamino)-2-((1R,3R,6R,8R,9R,10R,12R,13S,17S)-3-ethyl-10-methoxy-6,8,10,12,15,15,17-heptamethyl-5,7-dioxo-3',5'-dihydro-4,14,16-trioxaspiro[bicyclo[11.3.1]heptadecane-2,4'-pyrazole]-9-yloxy)-6-methyltetrahydro-2H-pyran-3-yl benzoate

(2S,3R,4S,6R)-4-(dimethylamino)-2-((1R,3R,6R,8R,9R,10R,12R,13S,17S)-3-ethyl-10-methoxy-3',6,8,10,12,15,15,17-octamethyl-5,7-dioxo-3',5'-dihydro-4,14,16-trioxaspiro[bicyclo[11.3.1]heptadecane-2,4'-pyrazole]-9-yloxy)-6-methyltetrahydro-2H-pyran-3-yl benzoate

(1R,3R,6R,8R,9R,10R,12R,13S,17S)-ethyl 9-((2S,3R,4S,6R)-3-(benzoyloxy)-4-(dimethylamino)-6-methyltetrahydro-2H-pyran-2-yloxy)-3-ethyl-10-methoxy-6,8,10,12,15,15,17-heptamethyl-5,7-dioxo-3',5'-dihydro-4,14,16-trioxaspiro[bicyclo[11.3.1]heptadecane-2,4'-pyrazole]-3'-carboxylate

(1R,3R,6R,8R,9R,10R,12R,13S,17S)-methyl-9-((2S,3R,4S,6R)-3-(benzoyloxy)-4-(dimethylamino)-6-methyltetrahydro-2H-pyran-2-yloxy)-3-ethyl-10-methoxy-6,8,10,12,15,15,17-heptamethyl-5,7-dioxo-3',5'-dihydro-4,14,16-trioxaspiro[bicyclo[11.3.1]heptadecane-2,4'-pyrazole]-3'-carboxylate

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