Technology Process of C25H30O3
There total 11 articles about C25H30O3 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
oxygen; palladium diacetate;
In
dimethyl sulfoxide;
at 20 - 80 ℃;
for 16h;
DOI:10.1002/ejoc.201101629
- Guidance literature:
-
With
pyridine; dihydrogen peroxide;
In
dichloromethane; water;
at 0 - 20 ℃;
for 0.25h;
DOI:10.1002/ejoc.201101629
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: methanol; diethyl ether; toluene / 0.25 h / Inert atmosphere
2.1: lithium aluminium tetrahydride / tetrahydrofuran; dichloromethane / 0.5 h / 0 °C / Inert atmosphere
3.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0.5 h / 0 °C / Inert atmosphere
3.2: 16 h / 20 °C / Inert atmosphere
4.1: toluene-4-sulfonic acid / water; acetone / 0.5 h / 20 °C
5.1: triethylamine / dichloromethane / 0.75 h / 0 °C / Inert atmosphere
6.1: oxygen; palladium diacetate / dimethyl sulfoxide / 16 h / 20 - 80 °C
With
lithium aluminium tetrahydride; oxygen; palladium diacetate; sodium hydride; toluene-4-sulfonic acid; triethylamine;
In
tetrahydrofuran; methanol; diethyl ether; dichloromethane; water; dimethyl sulfoxide; N,N-dimethyl-formamide; acetone; toluene; mineral oil;
DOI:10.1002/ejoc.201101629