C₃₁H₅₆O₅Si₂

Base Information

Chemical Name:C₃₁H₅₆O₅Si₂
CAS No.:1402820-49-8
Molecular Formula:C₃₁H₅₆O₅Si₂
Molecular Weight:564.954
Hs Code.:

C<sub>31</sub>H<sub>56</sub>O<sub>5</sub>Si<sub>2</sub>

Synonyms:C₃₁H₅₆O₅Si₂

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Chemical Property of C₃₁H₅₆O₅Si₂

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Technology Process of C₃₁H₅₆O₅Si₂

There total 1 articles about C₃₁H₅₆O₅Si₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: C₃₁H₅₈O₅Si₂

: 1402820-49-8
C₃₁H₅₆O₅Si₂

Guidance literature:: With tetrapropylammonium perruthennate; 4-methylmorpholine N-oxide; In dichloromethane; for 0.5h; Molecular sieve;
DOI:10.1002/anie.201203935

Reference yield:

: 1402820-49-8
C₃₁H₅₆O₅Si₂

: 1402820-27-2
C₃₁H₅₈O₅Si₂

: 1402820-26-1
C₃₁H₅₈O₅Si₂

Guidance literature:: With L-Selectride; In tetrahydrofuran; at -30 ℃; for 6h; optical yield given as %de;
DOI:10.1002/anie.201203935

Reference yield:

: 1402820-49-8
C₃₁H₅₆O₅Si₂

: C₂₈H₅₀O₇SSi

Guidance literature:: Multi-step reaction with 6 steps

1: L-Selectride / tetrahydrofuran / 6 h / -30 °C

2: pyridinium p-toluenesulfonate / diethyl ether / 14 h

3: lithium 4,4′-di(tert-butyl)biphenyl / tetrahydrofuran / 0.17 h / -78 °C

4: tributylphosphine / tetrahydrofuran / 16 h / 0 - 20 °C

5: 4-methylmorpholine N-oxide; tetrapropylammonium perruthennate / acetonitrile / 12 h / 20 °C

6: pyridine hydrogenfluoride / tetrahydrofuran / 24.5 h / 0 °C

With tetrapropylammonium perruthennate; lithium 4,4′-di(tert-butyl)biphenyl; tributylphosphine; pyridinium p-toluenesulfonate; L-Selectride; pyridine hydrogenfluoride; 4-methylmorpholine N-oxide; In tetrahydrofuran; diethyl ether; acetonitrile;
DOI:10.1021/ja404796n