1,3-di-tert-butyl-2[(Z)-1-ethyl-2-phenyl-2-trimethylstannylethenyl]2,3-dihydro-1H-1,3,2-diazaborole

Base Information

Chemical Name:1,3-di-tert-butyl-2[(Z)-1-ethyl-2-phenyl-2-trimethylstannylethenyl]2,3-dihydro-1H-1,3,2-diazaborole
CAS No.:287494-40-0
Molecular Formula:C₂₃H₃₉BN₂Sn
Molecular Weight:473.097
Hs Code.:

Synonyms:1,3-di-tert-butyl-2[(Z)-1-ethyl-2-phenyl-2-trimethylstannylethenyl]2,3-dihydro-1H-1,3,2-diazaborole

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Chemical Property of 1,3-di-tert-butyl-2[(Z)-1-ethyl-2-phenyl-2-trimethylstannylethenyl]2,3-dihydro-1H-1,3,2-diazaborole

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Technology Process of 1,3-di-tert-butyl-2[(Z)-1-ethyl-2-phenyl-2-trimethylstannylethenyl]2,3-dihydro-1H-1,3,2-diazaborole

There total 1 articles about 1,3-di-tert-butyl-2[(Z)-1-ethyl-2-phenyl-2-trimethylstannylethenyl]2,3-dihydro-1H-1,3,2-diazaborole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 222625-55-0
1,3-di-tert-butyl-2-trimethylstannyl-2,3-dihydro-1H-1,3,2-diazaborole

: 622-76-4,83585-27-7
1-phenyl-1-butyne

: 287494-40-0
1,3-di-tert-butyl-2[(Z)-1-ethyl-2-phenyl-2-trimethylstannylethenyl]2,3-dihydro-1H-1,3,2-diazaborole

Guidance literature:: tetrakis(triphenylphosphine) palladium⁽⁰⁾; In benzene; an equimolar amounts of alkyne was added to a soln. of borole and PdPh4in benzene at room temp., the mixt. was heated at 80°C for 2 h, cooled to room temp. (N2); volatiles was removed in vac., ppt. was dissolved in n-pentane, filtered, concd., stored at -30°C, recrystd. from n-pentane; elem. anal.;
DOI:10.1021/om000042w