Molybdenum, bis((1,2,3,4,5,6-eta)-1,3,5-trimethylbenzene)-

Base Information

Chemical Name:Molybdenum, bis((1,2,3,4,5,6-eta)-1,3,5-trimethylbenzene)-
CAS No.:12131-50-9
Molecular Formula:C₁₈H₂₄Mo
Molecular Weight:336.329
Hs Code.:

Synonyms:Molybdenum, bis((1,2,3,4,5,6-eta)-1,3,5-trimethylbenzene)-;Molybdenum,bis[(1,2,3,4,5,6-.eta.)-1,3,5-trimethylbenzene]-;12131-50-9

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Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Molybdenum, bis((1,2,3,4,5,6-eta)-1,3,5-trimethylbenzene)-

Chemical Property:

Vapor Pressure:2.32mmHg at 25°C
Boiling Point:166.7°C at 760 mmHg
Flash Point:44.4°C
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:6
Rotatable Bond Count:0
Exact Mass:338.093204
Heavy Atom Count:19
Complexity:227

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C[C-]1[CH-][C-]([CH-][C-]([CH-]1)C)C.CC1=CC(=CC(=C1)C)C.[Mo]

Technology Process of Molybdenum, bis((1,2,3,4,5,6-eta)-1,3,5-trimethylbenzene)-

There total 2 articles about Molybdenum, bis((1,2,3,4,5,6-eta)-1,3,5-trimethylbenzene)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 29.0%

: 10241-05-1
molybdenum(V) chloride

: 108-67-8
1,3,5-trimethyl-benzene

: 12131-50-9
Mo(1,3,5-trimethylbenzene)₂

Guidance literature:: With Al; AlCl₃; In tetrahydrofuran; 1,2-dimethoxyethane; (under Ar, Schlenk); flask charged with Al, AlCl3, ligand added, stirredat room temp. for 1 h, MoCl5 added, heated at 135°C for 30 h, co oled, mixt. of THF-DME added, refluxed for 6 h, cooled to room temp.; ppt. filtered, solvent removed in vacuo, ppt. dissolved in heptane, filtered, heptane stripped off, solid sublimed at 130°C/0.01 mmHg;
DOI:10.1039/b602783k

Reference yield:

: 108-67-8
1,3,5-trimethyl-benzene

: 7439-98-7
molybdenum

: 12131-50-9
Mo(1,3,5-trimethylbenzene)₂

Guidance literature:: co-condensation of Mo-atoms and vapor of org. compd. (-196°C); according to: F. W. S. Benfield, M. L. H. Green, J. S. Ogden, D. Young, J. Chem. Soc., Chem. Commun., (1973) 866; vac. sublimation;
DOI:10.1016/0022-328X(90)85410-Z