(Z)-2,3-dimethyl-2-butenyl p-methylphenyl sulfide-1,1,4,4,4-d5

Base Information

Chemical Name:(Z)-2,3-dimethyl-2-butenyl p-methylphenyl sulfide-1,1,4,4,4-d5
CAS No.:127130-10-3
Molecular Formula:C₁₃H₁₈S
Molecular Weight:211.312
Hs Code.:

Synonyms:(Z)-2,3-dimethyl-2-butenyl p-methylphenyl sulfide-1,1,4,4,4-d5

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (Z)-2,3-dimethyl-2-butenyl p-methylphenyl sulfide-1,1,4,4,4-d5

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Technology Process of (Z)-2,3-dimethyl-2-butenyl p-methylphenyl sulfide-1,1,4,4,4-d5

There total 5 articles about (Z)-2,3-dimethyl-2-butenyl p-methylphenyl sulfide-1,1,4,4,4-d5 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 10486-08-5
sodium p-thiocresolate

: 127130-36-3
(Z)-1-chloro-2,3-dimethyl-2-butene-1,1,4,4,4-d5

: 127130-10-3
(Z)-2,3-dimethyl-2-butenyl p-methylphenyl sulfide-1,1,4,4,4-d5

Guidance literature:: In ethanol; for 0.5h;
DOI:10.1021/ja00169a030

Reference yield:

: 766-39-2
2,3-Dimethylmaleic anhydride

: 127130-10-3
(Z)-2,3-dimethyl-2-butenyl p-methylphenyl sulfide-1,1,4,4,4-d5

Guidance literature:: Multi-step reaction with 5 steps

1: 76 percent / LiAlD₄ / diethyl ether / 3 h / 0 °C

2: 83 percent / N-chlorosuccinimide, methyl sulfide / CH₂Cl₂ / 1 h / 0 °C

3: 76 percent / LiAlD₄ / tetrahydrofuran / 6 h / Heating

4: N-chlorosuccinimide, methyl sulfide / CH₂Cl₂ / 1 h / 0 °C

5: 95 percent / ethanol / 0.5 h

With N-chloro-succinimide; lithium aluminium deuteride; dimethylsulfide; In tetrahydrofuran; diethyl ether; ethanol; dichloromethane;
DOI:10.1021/ja00169a030

Reference yield:

: 127130-34-1
(Z)-4-chloro-2,3-dimethyl-2-butenol-1,1,4,4-d4

: 127130-10-3
(Z)-2,3-dimethyl-2-butenyl p-methylphenyl sulfide-1,1,4,4,4-d5

Guidance literature:: Multi-step reaction with 3 steps

1: 76 percent / LiAlD₄ / tetrahydrofuran / 6 h / Heating

2: N-chlorosuccinimide, methyl sulfide / CH₂Cl₂ / 1 h / 0 °C

3: 95 percent / ethanol / 0.5 h

With N-chloro-succinimide; lithium aluminium deuteride; dimethylsulfide; In tetrahydrofuran; ethanol; dichloromethane;
DOI:10.1021/ja00169a030