5,7-Dihydroxy-1-(3,4,5-trimethoxy-benzyl)-3,4-dihydro-1H-isoquinoline-2-carbaldehyde

Base Information

Chemical Name:5,7-Dihydroxy-1-(3,4,5-trimethoxy-benzyl)-3,4-dihydro-1H-isoquinoline-2-carbaldehyde
CAS No.:84518-18-3
Molecular Formula:C₂₀H₂₃NO₆
Molecular Weight:373.406
Hs Code.:

Synonyms:5,7-Dihydroxy-1-(3,4,5-trimethoxy-benzyl)-3,4-dihydro-1H-isoquinoline-2-carbaldehyde

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Chemical Property of 5,7-Dihydroxy-1-(3,4,5-trimethoxy-benzyl)-3,4-dihydro-1H-isoquinoline-2-carbaldehyde

Chemical Property:

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Technology Process of 5,7-Dihydroxy-1-(3,4,5-trimethoxy-benzyl)-3,4-dihydro-1H-isoquinoline-2-carbaldehyde

There total 2 articles about 5,7-Dihydroxy-1-(3,4,5-trimethoxy-benzyl)-3,4-dihydro-1H-isoquinoline-2-carbaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 84423-16-5
5,7-dibenzyloxy-N-formyl-1-(3,4,5-trimethoxybenzyl)-1,2-dihydroisoquinoline

: 84518-18-3
5,7-Dihydroxy-1-(3,4,5-trimethoxy-benzyl)-3,4-dihydro-1H-isoquinoline-2-carbaldehyde

Guidance literature:: With hydrogen; palladium on activated charcoal; In tetrahydrofuran; water; at 60 ℃; for 22h; under 2427.2 Torr;
DOI:10.1248/cpb.30.3197

Reference yield:

: 84445-10-3
<α-(3,5-dibenzyloxyphenyl)-β-(3,4,5-trimethoxyphenyl)>-N-formyl-ethylaminoacetaldehyde diethyl acetal

: 84518-18-3
5,7-Dihydroxy-1-(3,4,5-trimethoxy-benzyl)-3,4-dihydro-1H-isoquinoline-2-carbaldehyde

Guidance literature:: Multi-step reaction with 2 steps

1: 100 percent / 1 N HCl / tetrahydrofuran / 0.5 h / Heating

2: H₂ / 10percent Pd-C / H₂O; tetrahydrofuran / 22 h / 60 °C / 2427.2 Torr

With hydrogenchloride; hydrogen; palladium on activated charcoal; In tetrahydrofuran; water;
DOI:10.1248/cpb.30.3197