[1-benzyl-2-(3-bromo-propionylamino)-3-phenyl-propyl]-carbamic acid cyclopentyl ester

Base Information

Chemical Name:[1-benzyl-2-(3-bromo-propionylamino)-3-phenyl-propyl]-carbamic acid cyclopentyl ester
CAS No.:922723-61-3
Molecular Formula:C₂₅H₃₁BrN₂O₃
Molecular Weight:487.437
Hs Code.:

Synonyms:[1-benzyl-2-(3-bromo-propionylamino)-3-phenyl-propyl]-carbamic acid cyclopentyl ester

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Chemical Property of [1-benzyl-2-(3-bromo-propionylamino)-3-phenyl-propyl]-carbamic acid cyclopentyl ester

Chemical Property:

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Technology Process of [1-benzyl-2-(3-bromo-propionylamino)-3-phenyl-propyl]-carbamic acid cyclopentyl ester

There total 9 articles about [1-benzyl-2-(3-bromo-propionylamino)-3-phenyl-propyl]-carbamic acid cyclopentyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 6921-34-2
benzylmagnesium chloride

: 922723-61-3
[1-benzyl-2-(3-bromo-propionylamino)-3-phenyl-propyl]-carbamic acid cyclopentyl ester

Guidance literature:: Multi-step reaction with 7 steps

1.1: CuBr*DMS / tetrahydrofuran / 0.17 h / -78 °C

1.2: tetrahydrofuran / -78 - 20 °C

2.1: 91 percent / Et₃N / CH₂Cl₂ / 0 - 20 °C

3.1: 64 percent / NaN₃ / dimethylformamide / 16 h / 60 °C

4.1: trifluoroacetic acid / CH₂Cl₂ / 0.5 h / 0 °C

5.1: triethanolamine / toluene; H₂O / 1 h / 20 °C

6.1: 99 percent / H₂ / Pd(OH)2/C

7.1: triethanolamine / toluene; H₂O / 0.5 h / 20 °C

With sodium azide; copper(I) bromide dimethylsulfide complex; triethanolamine; hydrogen; triethylamine; trifluoroacetic acid; palladium dihydroxide; In tetrahydrofuran; dichloromethane; water; N,N-dimethyl-formamide; toluene;
DOI:10.1021/jm060754+

Reference yield:

: 922723-30-6
2-azido-1-benzyl-3-phenyl-propylamine

: 922723-61-3
[1-benzyl-2-(3-bromo-propionylamino)-3-phenyl-propyl]-carbamic acid cyclopentyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: triethanolamine / toluene; H₂O / 1 h / 20 °C

2: 99 percent / H₂ / Pd(OH)2/C

3: triethanolamine / toluene; H₂O / 0.5 h / 20 °C

With triethanolamine; hydrogen; palladium dihydroxide; In water; toluene;
DOI:10.1021/jm060754+

Reference yield:

: 922722-32-5
(2-azido-1-benzyl-3-phenyl-propyl)-carbamic acid tert-butyl ester

: 922723-61-3
[1-benzyl-2-(3-bromo-propionylamino)-3-phenyl-propyl]-carbamic acid cyclopentyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: trifluoroacetic acid / CH₂Cl₂ / 0.5 h / 0 °C

2: triethanolamine / toluene; H₂O / 1 h / 20 °C

3: 99 percent / H₂ / Pd(OH)2/C

4: triethanolamine / toluene; H₂O / 0.5 h / 20 °C

With triethanolamine; hydrogen; trifluoroacetic acid; palladium dihydroxide; In dichloromethane; water; toluene;
DOI:10.1021/jm060754+