1-(3'-bromo-4'-((methoxymethoxy)methyl)phenylsulfonyl)-3-chlorobenzene

Base Information

Chemical Name:1-(3'-bromo-4'-((methoxymethoxy)methyl)phenylsulfonyl)-3-chlorobenzene
CAS No.:1222010-75-4
Molecular Formula:C₁₅H₁₄BrClO₄S
Molecular Weight:405.697
Hs Code.:

Synonyms:1-(3'-bromo-4'-((methoxymethoxy)methyl)phenylsulfonyl)-3-chlorobenzene

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Chemical Property of 1-(3'-bromo-4'-((methoxymethoxy)methyl)phenylsulfonyl)-3-chlorobenzene

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Technology Process of 1-(3'-bromo-4'-((methoxymethoxy)methyl)phenylsulfonyl)-3-chlorobenzene

There total 4 articles about 1-(3'-bromo-4'-((methoxymethoxy)methyl)phenylsulfonyl)-3-chlorobenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 1222010-74-3
(3-bromo-4-((methoxymethoxy)methyl)phenyl)(3-chlorophenyl)sulfane

: 1222010-75-4
1-(3'-bromo-4'-((methoxymethoxy)methyl)phenylsulfonyl)-3-chlorobenzene

Guidance literature:: (3-bromo-4-((methoxymethoxy)methyl)phenyl)(3-chlorophenyl)sulfane; With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; at 0 ℃; for 18h; Inert atmosphere;

With sodium hydroxide; In dichloromethane; Inert atmosphere;

Reference yield:

: 59142-68-6
2-bromo-4-fluorobenzaldehyde

: 1222010-75-4
1-(3'-bromo-4'-((methoxymethoxy)methyl)phenylsulfonyl)-3-chlorobenzene

Guidance literature:: Multi-step reaction with 4 steps

1.1: potassium carbonate / N,N-dimethyl-formamide / 0.5 h / 0 °C / Inert atmosphere

2.1: methanol; sodium tetrahydroborate / 0.5 h / 0 °C / Inert atmosphere

3.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 14 h / Inert atmosphere

4.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 18 h / 0 °C / Inert atmosphere

4.2: Inert atmosphere

With methanol; sodium tetrahydroborate; potassium carbonate; N-ethyl-N,N-diisopropylamine; 3-chloro-benzenecarboperoxoic acid; In dichloromethane; N,N-dimethyl-formamide;

Reference yield:

: 1222010-72-1
2-bromo-4-(3-chlorophenylsulfanyl)benzaldehyde

: 1222010-75-4
1-(3'-bromo-4'-((methoxymethoxy)methyl)phenylsulfonyl)-3-chlorobenzene

Guidance literature:: Multi-step reaction with 3 steps

1.1: methanol; sodium tetrahydroborate / 0.5 h / 0 °C / Inert atmosphere

2.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 14 h / Inert atmosphere

3.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 18 h / 0 °C / Inert atmosphere

3.2: Inert atmosphere

With methanol; sodium tetrahydroborate; N-ethyl-N,N-diisopropylamine; 3-chloro-benzenecarboperoxoic acid; In dichloromethane;