diphenyl 1--2-phenylethane-phosphonate

Base Information

Chemical Name:diphenyl 1--2-phenylethane-phosphonate
CAS No.:104130-96-3
Molecular Formula:C₂₈H₂₆NO₅P
Molecular Weight:487.492
Hs Code.:

diphenyl 1-<N-(benzyloxycarbonyl)amino>-2-phenylethane-phosphonate

Synonyms:diphenyl 1--2-phenylethane-phosphonate

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Chemical Property of diphenyl 1--2-phenylethane-phosphonate

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Technology Process of diphenyl 1--2-phenylethane-phosphonate

There total 1 articles about diphenyl 1--2-phenylethane-phosphonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 48.0%

: 101-02-0
triphenyl phosphite

: 621-84-1
O-benzyl carbamate

: 122-78-1
phenylacetaldehyde

: 104130-96-3
diphenyl 1--2-phenylethane-phosphonate

Guidance literature:: DOI:10.1021/jm00161a014

Reference yield: 85.0%

: 104130-96-3
diphenyl 1--2-phenylethane-phosphonate

: 88024-19-5
diphenyl 1-amino-2-phenylethanephosphonate hydrobromide

Guidance literature:: With hydrogen bromide; In acetic acid;
DOI:10.1021/jm00161a014

Reference yield:

: 104130-96-3
diphenyl 1--2-phenylethane-phosphonate

: {(S)-1-[1-(Dimethoxy-phosphanyloxy)-2-phenyl-ethylcarbamoyl]-ethyl}-carbamic acid benzyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 85 percent / HBr / acetic acid

2: CHCl₃ / Heating

3: potassium fluoride hydrate, 18-crown-6 / 0.08 h / Heating

With potassium fluoride; 18-crown-6 ether; hydrogen bromide; In chloroform; acetic acid;
DOI:10.1021/jm00161a014