4-O-(methyl 2',3',4'-tri-O-acetyl-β-D-glucopyranosyluronate)-2-hydroxy-6-pentadecanylbenzoic acid

Base Information

Chemical Name:4-O-(methyl 2',3',4'-tri-O-acetyl-β-D-glucopyranosyluronate)-2-hydroxy-6-pentadecanylbenzoic acid
CAS No.:869996-25-8
Molecular Formula:C₃₅H₅₂O₁₃
Molecular Weight:680.79
Hs Code.:

Synonyms:4-O-(methyl 2',3',4'-tri-O-acetyl-β-D-glucopyranosyluronate)-2-hydroxy-6-pentadecanylbenzoic acid

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Chemical Property of 4-O-(methyl 2',3',4'-tri-O-acetyl-β-D-glucopyranosyluronate)-2-hydroxy-6-pentadecanylbenzoic acid

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Technology Process of 4-O-(methyl 2',3',4'-tri-O-acetyl-β-D-glucopyranosyluronate)-2-hydroxy-6-pentadecanylbenzoic acid

There total 10 articles about 4-O-(methyl 2',3',4'-tri-O-acetyl-β-D-glucopyranosyluronate)-2-hydroxy-6-pentadecanylbenzoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 869996-23-6
benzyl 4-O-(methyl 2',3',4'-tri-O-acetyl-β-D-glucopyranosyluronate)-2-hydroxy-6-pentadecanylbenzoate

: 869996-25-8
4-O-(methyl 2',3',4'-tri-O-acetyl-β-D-glucopyranosyluronate)-2-hydroxy-6-pentadecanylbenzoic acid

Guidance literature:: With hydrogen; palladium on activated charcoal; In ethyl acetate; at 20 ℃; for 15h; under 760 Torr;
DOI:10.1021/jo051384k

Reference yield:

: 869996-15-6
benzyl 2,4-dihydroxy-6-pentadecanylbenzoate

: 869996-25-8
4-O-(methyl 2',3',4'-tri-O-acetyl-β-D-glucopyranosyluronate)-2-hydroxy-6-pentadecanylbenzoic acid

Guidance literature:: Multi-step reaction with 2 steps

1: Ag₂O / acetonitrile / 6 h / 38 °C

2: 89 mg / H₂ / Pd/C / ethyl acetate / 15 h / 20 °C / 760 Torr

With hydrogen; silver(l) oxide; palladium on activated charcoal; In ethyl acetate; acetonitrile; 1: Koenigs-Knorr reaction;
DOI:10.1021/jo051384k

Reference yield:

: 869996-09-8
2,4-bis(benzyloxy)-6-pentadecanylbenzoic acid

: 869996-25-8
4-O-(methyl 2',3',4'-tri-O-acetyl-β-D-glucopyranosyluronate)-2-hydroxy-6-pentadecanylbenzoic acid

Guidance literature:: Multi-step reaction with 4 steps

1: 99 percent / H₂ / Pd/C / ethyl acetate / 5 h / 20 °C / 760 Torr

2: 88 percent / KHCO₃ / dimethylformamide / 40 h / Heating

3: Ag₂O / acetonitrile / 6 h / 38 °C

4: 89 mg / H₂ / Pd/C / ethyl acetate / 15 h / 20 °C / 760 Torr

With hydrogen; potassium hydrogencarbonate; silver(l) oxide; palladium on activated charcoal; In ethyl acetate; N,N-dimethyl-formamide; acetonitrile; 3: Koenigs-Knorr reaction;
DOI:10.1021/jo051384k