2-(benzyl(tert-butoxycarbonyl)amino)-1-phenylethyl naphthalene-1-sulfonate

Base Information

Chemical Name:2-(benzyl(tert-butoxycarbonyl)amino)-1-phenylethyl naphthalene-1-sulfonate
CAS No.:1345985-94-5
Molecular Formula:C₃₀H₃₁NO₅S
Molecular Weight:517.646
Hs Code.:

Synonyms:2-(benzyl(tert-butoxycarbonyl)amino)-1-phenylethyl naphthalene-1-sulfonate

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Chemical Property of 2-(benzyl(tert-butoxycarbonyl)amino)-1-phenylethyl naphthalene-1-sulfonate

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Technology Process of 2-(benzyl(tert-butoxycarbonyl)amino)-1-phenylethyl naphthalene-1-sulfonate

There total 8 articles about 2-(benzyl(tert-butoxycarbonyl)amino)-1-phenylethyl naphthalene-1-sulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 85-46-1
1-Naphthalenesulfonyl chloride

: 215391-96-1
rac-2-(N-tert-Butoxycarbonyl-N-benzylamino)-1-phenylethanol

: 1345985-94-5
2-(benzyl(tert-butoxycarbonyl)amino)-1-phenylethyl naphthalene-1-sulfonate

Guidance literature:: rac-2-(N-tert-Butoxycarbonyl-N-benzylamino)-1-phenylethanol; With potassium hydroxide; In tetrahydrofuran; for 0.25h;

1-Naphthalenesulfonyl chloride; In tetrahydrofuran;
DOI:10.1016/j.bmcl.2011.08.078

Reference yield:

: 96-09-3
styrene oxide

: 1345985-94-5
2-(benzyl(tert-butoxycarbonyl)amino)-1-phenylethyl naphthalene-1-sulfonate

Guidance literature:: Multi-step reaction with 3 steps

1: activated silica / 24 h / Inert atmosphere

2: triethylamine / methanol / 0.5 h / Reflux

3: potassium hydroxide / tetrahydrofuran / 0.25 h

With triethylamine; potassium hydroxide; In tetrahydrofuran; methanol;
DOI:10.1016/j.bmcl.2011.08.078

Reference yield:

: 51096-49-2,91579-12-3,107171-75-5,27159-30-4
2-benzylamino-1-phenyl-ethanol

: 1345985-94-5
2-(benzyl(tert-butoxycarbonyl)amino)-1-phenylethyl naphthalene-1-sulfonate

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / methanol / 0.5 h / Reflux

2: potassium hydroxide / tetrahydrofuran / 0.25 h

With triethylamine; potassium hydroxide; In tetrahydrofuran; methanol;
DOI:10.1016/j.bmcl.2011.08.078