Technology Process of C37H36O2
There total 5 articles about C37H36O2 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
tetrabutyl ammonium fluoride;
In
tetrahydrofuran;
at 20 ℃;
for 0.5h;
DOI:10.1002/ejoc.201200655
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: sodium iodide; potassium carbonate / acetone / Reflux
2.1: triethylamine; bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide / tetrahydrofuran / 20 °C / Inert atmosphere
3.1: potassium hydroxide / methanol; tetrahydrofuran / 1 h
3.2: 48 h / 20 °C / Inert atmosphere
4.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 0.5 h / 20 °C
With
bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; tetrabutyl ammonium fluoride; potassium carbonate; triethylamine; sodium iodide; potassium hydroxide;
In
tetrahydrofuran; methanol; acetone;
2.1: |Sonogashira Cross-Coupling;
DOI:10.1002/ejoc.201200655
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: sulfuric acid; potassium iodide; dihydrogen peroxide / methanol / 2 h / 40 °C
2.1: sodium iodide; potassium carbonate / acetone / Reflux
3.1: triethylamine; bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide / tetrahydrofuran / 20 °C / Inert atmosphere
4.1: potassium hydroxide / methanol; tetrahydrofuran / 1 h
4.2: 48 h / 20 °C / Inert atmosphere
5.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 0.5 h / 20 °C
With
bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; sulfuric acid; tetrabutyl ammonium fluoride; dihydrogen peroxide; potassium carbonate; triethylamine; potassium iodide; sodium iodide; potassium hydroxide;
In
tetrahydrofuran; methanol; acetone;
3.1: |Sonogashira Cross-Coupling;
DOI:10.1002/ejoc.201200655