tert-butyl(tert-butoxycarbonylamino)(methyl(3-phenylprop-2-ynyl)amino)methylenecarbamate

Base Information

Chemical Name:tert-butyl(tert-butoxycarbonylamino)(methyl(3-phenylprop-2-ynyl)amino)methylenecarbamate
CAS No.:1268469-85-7
Molecular Formula:C₂₁H₂₉N₃O₄
Molecular Weight:387.479
Hs Code.:

Synonyms:tert-butyl(tert-butoxycarbonylamino)(methyl(3-phenylprop-2-ynyl)amino)methylenecarbamate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of tert-butyl(tert-butoxycarbonylamino)(methyl(3-phenylprop-2-ynyl)amino)methylenecarbamate

Chemical Property:

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Technology Process of tert-butyl(tert-butoxycarbonylamino)(methyl(3-phenylprop-2-ynyl)amino)methylenecarbamate

There total 3 articles about tert-butyl(tert-butoxycarbonylamino)(methyl(3-phenylprop-2-ynyl)amino)methylenecarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 34706-60-0
N-methyl-3-phenylprop-2-yn-1-amine

: 322474-21-5
N,N'-bis-Boc-S-methyl-isothiourea

: 1268469-85-7
tert-butyl(tert-butoxycarbonylamino)(methyl(3-phenylprop-2-ynyl)amino)methylenecarbamate

Guidance literature:: With triethylamine; mercury(II) oxide; In dichloromethane; at 20 ℃;
DOI:10.1002/anie.201006087

Reference yield:

: 60444-44-2
N-methyl-N-(3-phenylprop-2-yn-1-yl)prop-2-en-1-amine

: 1268469-85-7
tert-butyl(tert-butoxycarbonylamino)(methyl(3-phenylprop-2-ynyl)amino)methylenecarbamate

Guidance literature:: Multi-step reaction with 2 steps

1: tetrakis(triphenylphosphine) palladium⁽⁰⁾ / dichloromethane / 6 h / 20 °C / Inert atmosphere

2: triethylamine; mercury(II) oxide / dichloromethane / 20 °C

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; triethylamine; mercury(II) oxide; In dichloromethane;
DOI:10.1002/anie.201006087

Reference yield:

: 536-74-3
phenylacetylene

: 1268469-85-7
tert-butyl(tert-butoxycarbonylamino)(methyl(3-phenylprop-2-ynyl)amino)methylenecarbamate

Guidance literature:: Multi-step reaction with 3 steps

1: copper(I) bromide / acetonitrile / 22 h / 20 °C

2: tetrakis(triphenylphosphine) palladium⁽⁰⁾ / dichloromethane / 6 h / 20 °C / Inert atmosphere

3: triethylamine; mercury(II) oxide / dichloromethane / 20 °C

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; triethylamine; mercury(II) oxide; copper(I) bromide; In dichloromethane; acetonitrile;
DOI:10.1002/anie.201006087