4,5,6,7-tetrahydro-8-(1-methylethylidene)-1,3-diphenyl-4,7-methanoisobenzofuran

Base Information

• Chemical Name: 4,5,6,7-tetrahydro-8-(1-methylethylidene)-1,3-diphenyl-4,7-methanoisobenzofuran
• CAS No.: 401929-12-2
• Molecular Formula: C₂₄H₂₂O
• Molecular Weight: 326.438

Synonyms:4,5,6,7-tetrahydro-8-(1-methylethylidene)-1,3-diphenyl-4,7-methanoisobenzofuran

Chemical Property of 4,5,6,7-tetrahydro-8-(1-methylethylidene)-1,3-diphenyl-4,7-methanoisobenzofuran

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Technology Process of 4,5,6,7-tetrahydro-8-(1-methylethylidene)-1,3-diphenyl-4,7-methanoisobenzofuran

There total 1 articles about 4,5,6,7-tetrahydro-8-(1-methylethylidene)-1,3-diphenyl-4,7-methanoisobenzofuran which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

2,3-dibenzoyl-7-(1-methylethylidene)bicyclo[2.2.1]hept-2-ene (362050-13-3) → 4,5,6,7-tetrahydro-8-(1-methylethylidene)-1,3-diphenyl-4,7-methanoisobenzofuran (401929-12-2)

Guidance literature:

With triethyl phosphite; In 1,2-dichloro-benzene; for 1h; Heating;

DOI:10.1016/S0040-4020(01)00916-4

Reference yield: 96.0%

4,5,6,7-tetrahydro-8-(1-methylethylidene)-1,3-diphenyl-4,7-methanoisobenzofuran (401929-12-2) → (1R,7S,10S)-10-Bromo-10-isopropenyl-3,5-diphenyl-4-oxa-tricyclo[5.2.1.02,6]deca-2,5-diene

Guidance literature:

With N-Bromosuccinimide; In dichloromethane; at 20 ℃; for 0.333333h;

DOI:10.1016/S0040-4020(01)00916-4

Reference yield: 8.0%

4-Phenyl-1,2,4-triazolidine-3,5-dione (4233-33-4) + 4,5,6,7-tetrahydro-8-(1-methylethylidene)-1,3-diphenyl-4,7-methanoisobenzofuran (401929-12-2) → 1-((1R,7S,10R)-10-Isopropenyl-3,5-diphenyl-4-oxa-tricyclo[5.2.1.02,6]deca-2,5-dien-10-yl)-4-phenyl-[1,2,4]triazolidine-3,5-dione + 1-((1S,7R,10S)-10-Isopropenyl-3,5-diphenyl-4-oxa-tricyclo[5.2.1.02,6]deca-2,5-dien-10-yl)-4-phenyl-[1,2,4]triazolidine-3,5-dione

Guidance literature:

In dichloromethane; at 20 ℃; for 0.666667h;

DOI:10.1016/S0040-4020(01)00916-4

upstream raw materials:

2,3-dibenzoyl-7-(1-methylethylidene)bicyclo[2.2.1]hept-2-ene

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