3,6-bis(4,5-diphenyl-2H-imidazolyl-2-ylidene)-1,2,4,5-tetrafluorocyclohexa-1,4-diene

Base Information

Chemical Name:3,6-bis(4,5-diphenyl-2H-imidazolyl-2-ylidene)-1,2,4,5-tetrafluorocyclohexa-1,4-diene
CAS No.:713144-61-7
Molecular Formula:C₃₆H₂₀F₄N₄
Molecular Weight:584.575
Hs Code.:

Synonyms:3,6-bis(4,5-diphenyl-2H-imidazolyl-2-ylidene)-1,2,4,5-tetrafluorocyclohexa-1,4-diene

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Chemical Property of 3,6-bis(4,5-diphenyl-2H-imidazolyl-2-ylidene)-1,2,4,5-tetrafluorocyclohexa-1,4-diene

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Technology Process of 3,6-bis(4,5-diphenyl-2H-imidazolyl-2-ylidene)-1,2,4,5-tetrafluorocyclohexa-1,4-diene

There total 4 articles about 3,6-bis(4,5-diphenyl-2H-imidazolyl-2-ylidene)-1,2,4,5-tetrafluorocyclohexa-1,4-diene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 713144-58-2
1,4-bis(4,5-diphenylimidazolyl-2-yl)tetrafluorobenzene

: 713144-61-7
3,6-bis(4,5-diphenyl-2H-imidazolyl-2-ylidene)-1,2,4,5-tetrafluorocyclohexa-1,4-diene

Guidance literature:: With potassium hydroxide; potassium hexacyanoferrate(III); In benzene; at 20 ℃; for 24h;
DOI:10.1021/ja049423h

Reference yield:

: 3217-47-8
2,3,5,6-tetrafluoroterephthalaldehyde

: 713144-61-7
3,6-bis(4,5-diphenyl-2H-imidazolyl-2-ylidene)-1,2,4,5-tetrafluorocyclohexa-1,4-diene

Guidance literature:: Multi-step reaction with 2 steps

1: 20 percent / ammonium acetate; AcOH / 12 h / 130 °C

2: 92 percent / aq. KOH; K₃[Fe(CN)6] / benzene / 24 h / 20 °C

With ammonium acetate; potassium hydroxide; acetic acid; potassium hexacyanoferrate(III); In benzene;
DOI:10.1021/ja049423h

Reference yield:

: 327-54-8
1,2,4,5-Tetrafluorobenzene

: 713144-61-7
3,6-bis(4,5-diphenyl-2H-imidazolyl-2-ylidene)-1,2,4,5-tetrafluorocyclohexa-1,4-diene

Guidance literature:: Multi-step reaction with 4 steps

1: 65 percent / AlCl₃ / 12 h / 70 °C

2: 55 percent / FeSO₄*7H₂O; H₂SO₄ / 6 h / 150 °C

3: 20 percent / ammonium acetate; AcOH / 12 h / 130 °C

4: 92 percent / aq. KOH; K₃[Fe(CN)6] / benzene / 24 h / 20 °C

With ammonium acetate; potassium hydroxide; aluminium trichloride; sulfuric acid; iron(II) sulfate; acetic acid; potassium hexacyanoferrate(III); In benzene;
DOI:10.1021/ja049423h