[TBPY-5-15]-1,1,1,3,3,3-hexafluoro-2-{2-[1-butyl-3,3-bis(trifluoromethyl)-1,3-dihydro-2,1λ⁵-benzoxaphosphol-1-yl]phenyl}propan-2-ol

Base Information

• Chemical Name: [TBPY-5-15]-1,1,1,3,3,3-hexafluoro-2-{2-[1-butyl-3,3-bis(trifluoromethyl)-1,3-dihydro-2,1λ⁵-benzoxaphosphol-1-yl]phenyl}propan-2-ol
• CAS No.: 183946-56-7
• Molecular Formula: C₂₂H₁₉F₁₂O₂P
• Molecular Weight: 574.346

Synonyms:[TBPY-5-15]-1,1,1,3,3,3-hexafluoro-2-{2-[1-butyl-3,3-bis(trifluoromethyl)-1,3-dihydro-2,1λ⁵-benzoxaphosphol-1-yl]phenyl}propan-2-ol

Chemical Property of [TBPY-5-15]-1,1,1,3,3,3-hexafluoro-2-{2-[1-butyl-3,3-bis(trifluoromethyl)-1,3-dihydro-2,1λ⁵-benzoxaphosphol-1-yl]phenyl}propan-2-ol

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Technology Process of [TBPY-5-15]-1,1,1,3,3,3-hexafluoro-2-{2-[1-butyl-3,3-bis(trifluoromethyl)-1,3-dihydro-2,1λ⁵-benzoxaphosphol-1-yl]phenyl}propan-2-ol

There total 2 articles about [TBPY-5-15]-1,1,1,3,3,3-hexafluoro-2-{2-[1-butyl-3,3-bis(trifluoromethyl)-1,3-dihydro-2,1λ⁵-benzoxaphosphol-1-yl]phenyl}propan-2-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

n-butyllithium (109-72-8,29786-93-4) + (S)-3,3,3',3'-tetrakis(trifluoromethyl)-1,1'-spirobi<3H,2,1λ5-benzoxaphosphole> (77121-88-1) → [TBPY-5-15]-1,1,1,3,3,3-hexafluoro-2-{2-[1-butyl-3,3-bis(trifluoromethyl)-1,3-dihydro-2,1λ5-benzoxaphosphol-1-yl]phenyl}propan-2-ol (183946-56-7)

Guidance literature:

With hydrogenchloride; Yield given. Multistep reaction;

DOI:10.1021/ja9621408

Reference yield:

1-butyl-3,3,3',3'-tetrakis(trifluoromethyl)-1,1'-spirobi[1,3-dihydro-2,1λ5-benzoxaphosphole] (185069-60-7,183946-61-4) → [TBPY-5-15]-1,1,1,3,3,3-hexafluoro-2-{2-[1-butyl-3,3-bis(trifluoromethyl)-1,3-dihydro-2,1λ5-benzoxaphosphol-1-yl]phenyl}propan-2-ol (183946-56-7)

Guidance literature:

In toluene; at 39.9 ℃; Rate constant; Thermodynamic data; ΔH(excit.), ΔS(excit.); var. solvents;

DOI:10.1021/ja9621408

Reference yield:

[TBPY-5-15]-1,1,1,3,3,3-hexafluoro-2-{2-[1-butyl-3,3-bis(trifluoromethyl)-1,3-dihydro-2,1λ5-benzoxaphosphol-1-yl]phenyl}propan-2-ol (183946-56-7) → C6H4C(CF3)2OHPHOC(CF3)2C6H4CH(CH2)3(2-)*2Li(1+)

Guidance literature:

With n-butyllithium; In diethyl ether; at -78 ℃;

DOI:10.1021/ol015927y

upstream raw materials:

n-butyllithium

(S)-3,3,3',3'-tetrakis(trifluoromethyl)-1,1'-spirobi<3H,2,1λ⁵-benzoxaphosphole>

1-butyl-3,3,3',3'-tetrakis(trifluoromethyl)-1,1'-spirobi[1,3-dihydro-2,1λ⁵-benzoxaphosphole]

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