N,4-dimethyl-N-(4-(1-methyl-1H-indol-3-yl)-5-phenylfuran-2-yl)benzenesulfonamide

Base Information

Chemical Name:N,4-dimethyl-N-(4-(1-methyl-1H-indol-3-yl)-5-phenylfuran-2-yl)benzenesulfonamide
CAS No.:1562381-70-7
Molecular Formula:C₂₇H₂₄N₂O₃S
Molecular Weight:456.565
Hs Code.:

Synonyms:N,4-dimethyl-N-(4-(1-methyl-1H-indol-3-yl)-5-phenylfuran-2-yl)benzenesulfonamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N,4-dimethyl-N-(4-(1-methyl-1H-indol-3-yl)-5-phenylfuran-2-yl)benzenesulfonamide

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Technology Process of N,4-dimethyl-N-(4-(1-methyl-1H-indol-3-yl)-5-phenylfuran-2-yl)benzenesulfonamide

There total 17 articles about N,4-dimethyl-N-(4-(1-methyl-1H-indol-3-yl)-5-phenylfuran-2-yl)benzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 603-76-9
1-methylindole

: 1562381-58-1
4-hydroxy-N-methyl-N',4-diphenyl-N-tosylbut-2-ynimidamide

: 1562381-70-7
N,4-dimethyl-N-(4-(1-methyl-1H-indol-3-yl)-5-phenylfuran-2-yl)benzenesulfonamide

Guidance literature:: With boron trifluoride diethyl etherate; In acetonitrile; at 0 ℃; for 0.583333h; Inert atmosphere;
DOI:10.1021/ja412634w

Reference yield:

: 640-61-9
N-methyl-p-toluenesulfonylamide

: 1562381-70-7
N,4-dimethyl-N-(4-(1-methyl-1H-indol-3-yl)-5-phenylfuran-2-yl)benzenesulfonamide

Guidance literature:: Multi-step reaction with 4 steps

1.1: 1,10-Phenanthroline; potassium carbonate; copper(ll) sulfate pentahydrate / toluene / 80 °C / Inert atmosphere; Sealed tube

2.1: zinc trifluoromethanesulfonate / dichloromethane / 2.5 h / 50 °C / Inert atmosphere

3.1: diisopropylamine; zinc dibromide; trimethylsilyl trifluoromethanesulfonate / dichloromethane / 3 h / 20 °C / Inert atmosphere; Sealed tube

3.2: 0.5 h / 28 °C / Inert atmosphere; Sealed tube

4.1: boron trifluoride diethyl etherate / acetonitrile / 0.58 h / 0 °C / Inert atmosphere

With 1,10-Phenanthroline; copper(ll) sulfate pentahydrate; trimethylsilyl trifluoromethanesulfonate; boron trifluoride diethyl etherate; zinc trifluoromethanesulfonate; potassium carbonate; diisopropylamine; zinc dibromide; In dichloromethane; toluene; acetonitrile;
DOI:10.1021/ja412634w

Reference yield:

: 1562381-11-6
(E)-N-methyl-N-(4-phenylbut-3-en-1-yn-1-yl)methanesulfonamide

: 1562381-70-7
N,4-dimethyl-N-(4-(1-methyl-1H-indol-3-yl)-5-phenylfuran-2-yl)benzenesulfonamide

Guidance literature:: Multi-step reaction with 3 steps

1.1: silver(I) triflimide / 1,2-dichloro-ethane / 15 h / 28 °C / Inert atmosphere

2.1: diisopropylamine; zinc dibromide; trimethylsilyl trifluoromethanesulfonate / dichloromethane / 3 h / 20 °C / Inert atmosphere; Sealed tube

2.2: 0.5 h / 28 °C / Inert atmosphere; Sealed tube

3.1: boron trifluoride diethyl etherate / acetonitrile / 0.58 h / 0 °C / Inert atmosphere

With trimethylsilyl trifluoromethanesulfonate; boron trifluoride diethyl etherate; diisopropylamine; zinc dibromide; silver(I) triflimide; In dichloromethane; 1,2-dichloro-ethane; acetonitrile;
DOI:10.1021/ja412634w