N'-benzyl-N-[carbomethoxy(methoxy)methyl]-N-methyl-N'-phenylethyl-1,2-diamine

Base Information

• Chemical Name: N'-benzyl-N-[carbomethoxy(methoxy)methyl]-N-methyl-N'-phenylethyl-1,2-diamine
• CAS No.: 1258726-89-4
• Molecular Formula: C₂₀H₂₆N₂O₃
• Molecular Weight: 342.438

Synonyms:N'-benzyl-N-[carbomethoxy(methoxy)methyl]-N-methyl-N'-phenylethyl-1,2-diamine

Chemical Property of N'-benzyl-N-[carbomethoxy(methoxy)methyl]-N-methyl-N'-phenylethyl-1,2-diamine

Chemical Property:

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Technology Process of N'-benzyl-N-[carbomethoxy(methoxy)methyl]-N-methyl-N'-phenylethyl-1,2-diamine

There total 1 articles about N'-benzyl-N-[carbomethoxy(methoxy)methyl]-N-methyl-N'-phenylethyl-1,2-diamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

methyl methoxybromoacetate (5193-96-4) + N-benzyl-N'-methyl-N-phenylethylenediamine (66711-48-6) → N'-benzyl-N-[carbomethoxy(methoxy)methyl]-N-methyl-N'-phenylethyl-1,2-diamine (1258726-89-4)

Guidance literature:

With N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; at 20 ℃; for 1h; Inert atmosphere;

DOI:10.1016/j.tet.2010.09.077

Reference yield: 89.0%

N'-benzyl-N-[carbomethoxy(methoxy)methyl]-N-methyl-N'-phenylethyl-1,2-diamine (1258726-89-4) → 1-benzyl-5-carbomethoxy-4-methyl-2,3,4,5-tetrahydro-1H-1,4-benzodiazepine (1258727-37-5)

Guidance literature:

With chloro-trimethyl-silane; In dichloromethane; at 20 ℃; for 0.5h; Inert atmosphere;

DOI:10.1016/j.tet.2010.09.077

upstream raw materials:

methyl methoxybromoacetate

N-benzyl-N'-methyl-N-phenylethylenediamine

Downstream raw materials:

1-benzyl-5-carbomethoxy-4-methyl-2,3,4,5-tetrahydro-1H-1,4-benzodiazepine

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