Phthalic acid mono-[(R)-1-(2-methoxycarbonyl-ethyl)-undec-2-ynyl] ester; compound with (R)-1-phenyl-ethylamine

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Chemical Name:Phthalic acid mono-[(R)-1-(2-methoxycarbonyl-ethyl)-undec-2-ynyl] ester; compound with (R)-1-phenyl-ethylamine
CAS No.:81793-48-8
Molecular Formula:C₈H₁₁N*C₂₃H₃₀O₆
Molecular Weight:523.67
Hs Code.:

Synonyms:Phthalic acid mono-[(R)-1-(2-methoxycarbonyl-ethyl)-undec-2-ynyl] ester; compound with (R)-1-phenyl-ethylamine

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Chemical Property of Phthalic acid mono-[(R)-1-(2-methoxycarbonyl-ethyl)-undec-2-ynyl] ester; compound with (R)-1-phenyl-ethylamine

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Technology Process of Phthalic acid mono-[(R)-1-(2-methoxycarbonyl-ethyl)-undec-2-ynyl] ester; compound with (R)-1-phenyl-ethylamine

There total 3 articles about Phthalic acid mono-[(R)-1-(2-methoxycarbonyl-ethyl)-undec-2-ynyl] ester; compound with (R)-1-phenyl-ethylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 764-93-2
1-decyne

: 81793-48-8
Phthalic acid mono-[(R)-1-(2-methoxycarbonyl-ethyl)-undec-2-ynyl] ester; compound with (R)-1-phenyl-ethylamine

Guidance literature:: Multi-step reaction with 3 steps

1: Mg / tetrahydrofuran / 1 h / Heating

2: 68 percent / tetrahydrofuran / -65 deg C, 3 h -> room temperature, 20 h

3: 1.) 9-BBN, (+)-α-pinene, 2.) 2-hydroxyethylamine, 3.) pyridine

With pyridine; 9-borabicyclo[3.3.1]nonane dimer; 2,6,6-trimethylbicyclo[3.1.1]hept-2-ene; magnesium; ethanolamine; In tetrahydrofuran;

Reference yield:

: 52713-82-3
dec-1-yn-1-ylmagnesium bromide

: 81793-48-8
Phthalic acid mono-[(R)-1-(2-methoxycarbonyl-ethyl)-undec-2-ynyl] ester; compound with (R)-1-phenyl-ethylamine

Guidance literature:: Multi-step reaction with 2 steps

1: 68 percent / tetrahydrofuran / -65 deg C, 3 h -> room temperature, 20 h

2: 1.) 9-BBN, (+)-α-pinene, 2.) 2-hydroxyethylamine, 3.) pyridine

With pyridine; 9-borabicyclo[3.3.1]nonane dimer; 2,6,6-trimethylbicyclo[3.1.1]hept-2-ene; ethanolamine; In tetrahydrofuran;

Reference yield:

: 85-44-9
phthalic anhydride

: 3886-69-9
(+)-1-phenylethylamine

: 77889-02-2
methyl 4-oxo-5-tetradecyonate

: 81793-48-8
Phthalic acid mono-[(R)-1-(2-methoxycarbonyl-ethyl)-undec-2-ynyl] ester; compound with (R)-1-phenyl-ethylamine

Guidance literature:: With pyridine; 9-borabicyclo[3.3.1]nonane dimer; 2,6,6-trimethylbicyclo[3.1.1]hept-2-ene; ethanolamine; Yield given. Multistep reaction;