N-benzyloxy-N-carbethoxy-1-carboxy-2,3-O-isopropylidene-β-D-erythrofuranosylamine

Base Information

• Chemical Name: N-benzyloxy-N-carbethoxy-1-carboxy-2,3-O-isopropylidene-β-D-erythrofuranosylamine
• CAS No.: 170590-75-7
• Molecular Formula: C₁₈H₂₃NO₈
• Molecular Weight: 381.383

Synonyms:N-benzyloxy-N-carbethoxy-1-carboxy-2,3-O-isopropylidene-β-D-erythrofuranosylamine

Chemical Property of N-benzyloxy-N-carbethoxy-1-carboxy-2,3-O-isopropylidene-β-D-erythrofuranosylamine

Chemical Property:

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Technology Process of N-benzyloxy-N-carbethoxy-1-carboxy-2,3-O-isopropylidene-β-D-erythrofuranosylamine

There total 1 articles about N-benzyloxy-N-carbethoxy-1-carboxy-2,3-O-isopropylidene-β-D-erythrofuranosylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N-benzyloxy-N-carbethoxy-1-formyl-2,3-O-isopropylidene-β-D-erythrofuranosylamine → N-benzyloxy-N-carbethoxy-1-carboxy-2,3-O-isopropylidene-β-D-erythrofuranosylamine (170590-75-7)

Guidance literature:

With sodium chlorite; camphor-10-sulfonic acid; In water; tert-butyl alcohol; for 3h; Yield given;

DOI:10.1016/0040-4020(95)00324-2

Reference yield: 95.0%

diazomethane (186581-53-3,908094-01-9,334-88-3) + N-benzyloxy-N-carbethoxy-1-carboxy-2,3-O-isopropylidene-β-D-erythrofuranosylamine (170590-75-7) → N-benzyloxy-N-carbethoxy-1-carbomethoxy-2,3-O-isopropylidene-β-D-erythrofuranosylamine

Guidance literature:

In dichloromethane; at 0 ℃;

DOI:10.1016/0040-4020(95)00324-2

Reference yield:

N-benzyloxy-N-carbethoxy-1-carboxy-2,3-O-isopropylidene-β-D-erythrofuranosylamine (170590-75-7) → N-benzyloxy-N-carbethoxy-1-carbamoyl-2,3-O-isopropylidene-β-D-erythrofuranosylamine

Guidance literature:

With ammonia; bromo-tris(1-pyrrolidinyl)phosphonium hexafluorophosphate; In dichloromethane; for 0.75h;

DOI:10.1016/0040-4020(95)00324-2

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