3-{4-[2-(N-nonyl-N-pyridin-2-ylamino)ethoxy]phenyl}-2-methylpropanoic acid methyl ester

Base Information

Chemical Name:3-{4-[2-(N-nonyl-N-pyridin-2-ylamino)ethoxy]phenyl}-2-methylpropanoic acid methyl ester
CAS No.:952481-13-9
Molecular Formula:C₂₇H₄₀N₂O₃
Molecular Weight:440.626
Hs Code.:

Synonyms:3-{4-[2-(N-nonyl-N-pyridin-2-ylamino)ethoxy]phenyl}-2-methylpropanoic acid methyl ester

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Chemical Property of 3-{4-[2-(N-nonyl-N-pyridin-2-ylamino)ethoxy]phenyl}-2-methylpropanoic acid methyl ester

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Technology Process of 3-{4-[2-(N-nonyl-N-pyridin-2-ylamino)ethoxy]phenyl}-2-methylpropanoic acid methyl ester

There total 7 articles about 3-{4-[2-(N-nonyl-N-pyridin-2-ylamino)ethoxy]phenyl}-2-methylpropanoic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 11.0%

: 952481-11-7
3-[4-(2-bromoethoxy)phenyl]-2-methylpropionic acid methyl ester

: 850724-06-0
2-(nonylamino)pyridine

: 952481-13-9
3-{4-[2-(N-nonyl-N-pyridin-2-ylamino)ethoxy]phenyl}-2-methylpropanoic acid methyl ester

Guidance literature:: With triethylamine; potassium iodide; In tetrahydrofuran; at 105 ℃; for 28h;
DOI:10.1248/cpb.55.1053

Reference yield:

: 109-04-6
2-bromo-pyridine

: 952481-13-9
3-{4-[2-(N-nonyl-N-pyridin-2-ylamino)ethoxy]phenyl}-2-methylpropanoic acid methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 70 percent / rac-BINAP; sodium tert-butoxide / Pd₂(DBA)3 / toluene / 72 h / 105 °C

2: 11 percent / KI; Et₃N / tetrahydrofuran / 28 h / 105 °C

With 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; triethylamine; potassium iodide; sodium t-butanolate; tris(dibenzylideneacetone)dipalladium ⁽⁰⁾; In tetrahydrofuran; toluene;
DOI:10.1248/cpb.55.1053

Reference yield:

: 112-20-9
n-Nonylamin

: 952481-13-9
3-{4-[2-(N-nonyl-N-pyridin-2-ylamino)ethoxy]phenyl}-2-methylpropanoic acid methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 70 percent / rac-BINAP; sodium tert-butoxide / Pd₂(DBA)3 / toluene / 72 h / 105 °C

2: 11 percent / KI; Et₃N / tetrahydrofuran / 28 h / 105 °C

With 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; triethylamine; potassium iodide; sodium t-butanolate; tris(dibenzylideneacetone)dipalladium ⁽⁰⁾; In tetrahydrofuran; toluene;
DOI:10.1248/cpb.55.1053