Technology Process of C16H15N3O3S
There total 6 articles about C16H15N3O3S which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
methanol; hydrazine hydrate;
at 20 - 40 ℃;
for 17h;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: borane-THF / tetrahydrofuran / 4 h / 0 - 20 °C
2: acetone / 1 h / 20 °C
3: 1-chloro-1-(dimethylamino)-2-methyl-1-propene / dichloromethane / 2 h / 20 °C
4: hydrazine hydrate; methanol / 17 h / 20 - 40 °C
With
methanol; borane-THF; 1-chloro-1-(dimethylamino)-2-methyl-1-propene; hydrazine hydrate;
In
tetrahydrofuran; dichloromethane; acetone;
- Guidance literature:
-
Multi-step reaction with 6 steps
1: sulfuric acid; acetic acid / 2 h / 20 °C
2: thiourea; acetic acid / ethanol / 80 °C
3: borane-THF / tetrahydrofuran / 4 h / 0 - 20 °C
4: acetone / 1 h / 20 °C
5: 1-chloro-1-(dimethylamino)-2-methyl-1-propene / dichloromethane / 2 h / 20 °C
6: hydrazine hydrate; methanol / 17 h / 20 - 40 °C
With
methanol; borane-THF; 1-chloro-1-(dimethylamino)-2-methyl-1-propene; sulfuric acid; hydrazine hydrate; acetic acid; thiourea;
In
tetrahydrofuran; ethanol; dichloromethane; acetone;