2-(1,5-bis(benzyloxy)-4-oxo-1,4-dihydropyridine-2-carboxamido)acetic acid

Base Information

Chemical Name:2-(1,5-bis(benzyloxy)-4-oxo-1,4-dihydropyridine-2-carboxamido)acetic acid
CAS No.:1380111-37-4
Molecular Formula:C₂₂H₂₀N₂O₆
Molecular Weight:408.411
Hs Code.:

Synonyms:2-(1,5-bis(benzyloxy)-4-oxo-1,4-dihydropyridine-2-carboxamido)acetic acid

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Chemical Property of 2-(1,5-bis(benzyloxy)-4-oxo-1,4-dihydropyridine-2-carboxamido)acetic acid

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Technology Process of 2-(1,5-bis(benzyloxy)-4-oxo-1,4-dihydropyridine-2-carboxamido)acetic acid

There total 3 articles about 2-(1,5-bis(benzyloxy)-4-oxo-1,4-dihydropyridine-2-carboxamido)acetic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1380111-36-3
C₂₆H₂₈N₂O₆

: 1380111-37-4
2-(1,5-bis(benzyloxy)-4-oxo-1,4-dihydropyridine-2-carboxamido)acetic acid

Guidance literature:: C₂₆H₂₈N₂O₆; With formic acid; at 20 - 50 ℃;

With sodium hydrogencarbonate; In water; ethyl acetate; pH=9;

Reference yield:

: methyl 2-(1,5-bis(benzyloxy)-4-oxo-1,4-dihydropyridine-2-carboxamido)acetate

: 1380111-37-4
2-(1,5-bis(benzyloxy)-4-oxo-1,4-dihydropyridine-2-carboxamido)acetic acid

Guidance literature:: With water; sodium hydroxide; In tetrahydrofuran; at 0 ℃; for 4h;
DOI:10.1021/jm501506f

Reference yield:

: 1380109-89-6
1,5-bis(benzyloxy)-4-oxo-1,4-dihydropyridine-2-carboxylic acid

: 1380111-37-4
2-(1,5-bis(benzyloxy)-4-oxo-1,4-dihydropyridine-2-carboxamido)acetic acid

Guidance literature:: Multi-step reaction with 2 steps

1: N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 20 °C

2: sodium hydroxide; water / tetrahydrofuran / 4 h / 0 °C

With water; N-ethyl-N,N-diisopropylamine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate; sodium hydroxide; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1021/jm501506f