3-(3-(4,5-dimethoxy-2-methyl-3,6-dioxocyclohexa-1,4-dienyl)propoxy)propyl nitrate

Base Information

Chemical Name:3-(3-(4,5-dimethoxy-2-methyl-3,6-dioxocyclohexa-1,4-dienyl)propoxy)propyl nitrate
CAS No.:1431987-04-0
Molecular Formula:C₁₅H₂₁NO₈
Molecular Weight:343.334
Hs Code.:

Synonyms:3-(3-(4,5-dimethoxy-2-methyl-3,6-dioxocyclohexa-1,4-dienyl)propoxy)propyl nitrate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-(3-(4,5-dimethoxy-2-methyl-3,6-dioxocyclohexa-1,4-dienyl)propoxy)propyl nitrate

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Technology Process of 3-(3-(4,5-dimethoxy-2-methyl-3,6-dioxocyclohexa-1,4-dienyl)propoxy)propyl nitrate

There total 7 articles about 3-(3-(4,5-dimethoxy-2-methyl-3,6-dioxocyclohexa-1,4-dienyl)propoxy)propyl nitrate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 1448013-69-1
3-[3-(2,3,4,5-tetramethoxy-6-methylphenyl)propoxy]propyl nitrate

: 1431987-04-0
3-(3-(4,5-dimethoxy-2-methyl-3,6-dioxocyclohexa-1,4-dienyl)propoxy)propyl nitrate

Guidance literature:: With ammonium cerium (IV) nitrate; In water; acetonitrile; at 0 ℃; for 3h;

Reference yield: 29.0%

: 1431987-57-3
3-[3-(2,3,4,5-tetramethoxy-6-methylphenyl)propoxy]propanol

: 1431987-04-0
3-(3-(4,5-dimethoxy-2-methyl-3,6-dioxocyclohexa-1,4-dienyl)propoxy)propyl nitrate

: 1448013-69-1
3-[3-(2,3,4,5-tetramethoxy-6-methylphenyl)propoxy]propyl nitrate

Guidance literature:: With 2,6-di-tert-butyl-4-methylpyridine; trifluoromethylsulfonic anhydride; tetrabutylammonium nitrate; In dichloromethane; at -78 ℃; for 0.5h;

Reference yield:

: 71573-66-5
1‐allyl‐2,3,4,5‐tetramethoxy‐6‐methylbenzene

: 1431987-04-0
3-(3-(4,5-dimethoxy-2-methyl-3,6-dioxocyclohexa-1,4-dienyl)propoxy)propyl nitrate

Guidance literature:: Multi-step reaction with 6 steps

1.1: 9-bora-bicyclo[3.3.1]nonane / tetrahydrofuran / 16 h / 0 - 20 °C

1.2: 0.5 h / 0 °C

2.1: triethylamine; dmap / dichloromethane / 5 h / 0 °C

3.1: sodium hydride / tetrahydrofuran; mineral oil / 0.17 h

3.2: 70 °C

4.1: 9-bora-bicyclo[3.3.1]nonane / tetrahydrofuran / 18 h / 0 - 20 °C

4.2: 0.5 h

5.1: 2,6-di-tert-butyl-4-methylpyridine; tetrabutylammonium nitrate; trifluoromethylsulfonic anhydride / dichloromethane / 0.5 h / -78 °C

6.1: ammonium cerium (IV) nitrate / acetonitrile; water / 3 h / 0 °C

With dmap; 2,6-di-tert-butyl-4-methylpyridine; ammonium cerium (IV) nitrate; trifluoromethylsulfonic anhydride; tetrabutylammonium nitrate; sodium hydride; triethylamine; 9-bora-bicyclo[3.3.1]nonane; In tetrahydrofuran; dichloromethane; water; acetonitrile; mineral oil;