5,6,7,8-tetraphenyl-3a,4,4a,8a,9,9a-hexahydro-4,9-methano-1H-benz{f}indene

Base Information

Chemical Name:5,6,7,8-tetraphenyl-3a,4,4a,8a,9,9a-hexahydro-4,9-methano-1H-benz{f}indene
CAS No.:113567-78-5
Molecular Formula:C₃₈H₃₂
Molecular Weight:488.672
Hs Code.:

Synonyms:5,6,7,8-tetraphenyl-3a,4,4a,8a,9,9a-hexahydro-4,9-methano-1H-benz{f}indene

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Chemical Property of 5,6,7,8-tetraphenyl-3a,4,4a,8a,9,9a-hexahydro-4,9-methano-1H-benz{f}indene

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Technology Process of 5,6,7,8-tetraphenyl-3a,4,4a,8a,9,9a-hexahydro-4,9-methano-1H-benz{f}indene

There total 2 articles about 5,6,7,8-tetraphenyl-3a,4,4a,8a,9,9a-hexahydro-4,9-methano-1H-benz{f}indene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: copper(II) choride dihydrate

: 113626-31-6
(5,6,7,8-η4-5,6,7,8-tetraphenyl-3a,4,4a,8a,9,9a-endo-hexahydro-4,9-methano-1H-benz{f}indene)(η5-cyclopentadienyl)cobalt

: 113567-78-5
5,6,7,8-tetraphenyl-3a,4,4a,8a,9,9a-hexahydro-4,9-methano-1H-benz{f}indene

Guidance literature:: With triethylamine; In acetonitrile; Addn. of CuCl2*2H2O to soln. of complex under N2 at 0°C, stirring (30 min).; Addn. of H2O, extg. (hexane), evapn. of solvent in vac., filtn. through Al2O3, evapn. of solvent.;

Reference yield: 37.0%

: copper(II) choride dihydrate

: 113567-74-1
(5,6,7,8-η4-5,6,7,8-tetraphenyl-3a,4,4a,8a,9,9a-exo-hexahydro-4,9-methano-1H-benz{f}indene)(η5-cyclopentadienyl)cobalt

: 113567-78-5
5,6,7,8-tetraphenyl-3a,4,4a,8a,9,9a-hexahydro-4,9-methano-1H-benz{f}indene

Guidance literature:: With triethylamine; In acetonitrile; Addn. of CuCl2*2H2O to soln. of complex under N2 at 0°C, stirring (30 min).; Addn. of H2O, extg. (hexane), evapn. of solvent in vac., filtn. through Al2O3, evapn. of solvent.;