Diazo-acetic acid (3aR,4R,6S,6aR)-2,2-dimethyl-6-phenylsulfanyl-tetrahydro-furo[3,4-d][1,3]dioxol-4-ylmethyl ester

Base Information

Chemical Name:Diazo-acetic acid (3aR,4R,6S,6aR)-2,2-dimethyl-6-phenylsulfanyl-tetrahydro-furo[3,4-d][1,3]dioxol-4-ylmethyl ester
CAS No.:153362-33-5
Molecular Formula:C₁₆H₁₈N₂O₅S
Molecular Weight:350.395
Hs Code.:

Synonyms:Diazo-acetic acid (3aR,4R,6S,6aR)-2,2-dimethyl-6-phenylsulfanyl-tetrahydro-furo[3,4-d][1,3]dioxol-4-ylmethyl ester

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Chemical Property of Diazo-acetic acid (3aR,4R,6S,6aR)-2,2-dimethyl-6-phenylsulfanyl-tetrahydro-furo[3,4-d][1,3]dioxol-4-ylmethyl ester

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Technology Process of Diazo-acetic acid (3aR,4R,6S,6aR)-2,2-dimethyl-6-phenylsulfanyl-tetrahydro-furo[3,4-d][1,3]dioxol-4-ylmethyl ester

There total 4 articles about Diazo-acetic acid (3aR,4R,6S,6aR)-2,2-dimethyl-6-phenylsulfanyl-tetrahydro-furo[3,4-d][1,3]dioxol-4-ylmethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 14661-69-9
p-toluenesulfonylhydrazone glyoxylic acid chloride

: 153362-34-6
β-phenylthio-2,3-O-isopropylidene-D-ribofuranose

: 153362-33-5
Diazo-acetic acid (3aR,4R,6S,6aR)-2,2-dimethyl-6-phenylsulfanyl-tetrahydro-furo[3,4-d][1,3]dioxol-4-ylmethyl ester

Guidance literature:: DOI:10.1016/S0040-4039(00)60417-3

Reference yield:

: 4551-15-9
phenylthiotrimethylsilane

: 153362-33-5
Diazo-acetic acid (3aR,4R,6S,6aR)-2,2-dimethyl-6-phenylsulfanyl-tetrahydro-furo[3,4-d][1,3]dioxol-4-ylmethyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: 97 percent / BF₃OEt₂ / CH₂Cl₂

2: 98 percent / ammonia / methanol

3: 83 percent / CuSO₄, H₂SO₄

4: 94 percent

With sulfuric acid; boron trifluoride diethyl etherate; ammonia; copper(II) sulfate; In methanol; dichloromethane;
DOI:10.1016/S0040-4039(00)60417-3

Reference yield:

: 52544-88-4
phenyl 2,3,5-tri-O-acetyl-1-thio-β-D-ribofuranoside

: 153362-33-5
Diazo-acetic acid (3aR,4R,6S,6aR)-2,2-dimethyl-6-phenylsulfanyl-tetrahydro-furo[3,4-d][1,3]dioxol-4-ylmethyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 98 percent / ammonia / methanol

2: 83 percent / CuSO₄, H₂SO₄

3: 94 percent

With sulfuric acid; ammonia; copper(II) sulfate; In methanol;
DOI:10.1016/S0040-4039(00)60417-3