(1R)-2-((4-aminobutyl){[(1-methylethyl)amino]carbonyl}amino)-1-[(methyloxy)methyl]ethyl phenylcarbamate trifluoroacetate

Base Information

• Chemical Name: (1R)-2-((4-aminobutyl){[(1-methylethyl)amino]carbonyl}amino)-1-[(methyloxy)methyl]ethyl phenylcarbamate trifluoroacetate
• CAS No.: 1203704-81-7
• Molecular Formula: C₂HF₃O₂*C₁₉H₃₂N₄O₄
• Molecular Weight: 494.511

Synonyms:(1R)-2-((4-aminobutyl){[(1-methylethyl)amino]carbonyl}amino)-1-[(methyloxy)methyl]ethyl phenylcarbamate trifluoroacetate

Chemical Property of (1R)-2-((4-aminobutyl){[(1-methylethyl)amino]carbonyl}amino)-1-[(methyloxy)methyl]ethyl phenylcarbamate trifluoroacetate

Chemical Property:

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Technology Process of (1R)-2-((4-aminobutyl){[(1-methylethyl)amino]carbonyl}amino)-1-[(methyloxy)methyl]ethyl phenylcarbamate trifluoroacetate

There total 1 articles about (1R)-2-((4-aminobutyl){[(1-methylethyl)amino]carbonyl}amino)-1-[(methyloxy)methyl]ethyl phenylcarbamate trifluoroacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1,1-dimethylethyl {4-[{[(1-methylethyl)amino]carbonyl}((2R)-3-(methyloxy)-2-{[(phenylamino)carbonyl]oxy}propyl)amino]butyl}carbamate (929282-27-9) + trifluoroacetic acid (76-05-1) → (1R)-2-((4-aminobutyl){[(1-methylethyl)amino]carbonyl}amino)-1-[(methyloxy)methyl]ethyl phenylcarbamate trifluoroacetate (1203704-81-7)

Guidance literature:

In dichloromethane; at 20 ℃; for 4h;

Reference yield: 65.0%

(1R)-2-((4-aminobutyl){[(1-methylethyl)amino]carbonyl}amino)-1-[(methyloxy)methyl]ethyl phenylcarbamate trifluoroacetate (1203704-81-7) + 2-chloro-4-fluorobenzene-1-sulfonyl chloride (85958-57-2) → (1R)-2-((4-{[(2-chloro-4-fluorophenyl)sulfonyl]amino}butyl){[(1-methylethyl)amino]carbonyl}amino)-1-[(methyloxy)methyl]ethyl phenylcarbamate (929281-12-9)

Guidance literature:

With triethylamine; In dichloromethane; at 20 ℃; for 5h;

upstream raw materials:

1,1-dimethylethyl {4-[{[(1-methylethyl)amino]carbonyl}((2R)-3-(methyloxy)-2-{[(phenylamino)carbonyl]oxy}propyl)amino]butyl}carbamate

trifluoroacetic acid

Downstream raw materials:

(1R)-2-((4-{[(2-chloro-4-fluorophenyl)sulfonyl]amino}butyl){[(1-methylethyl)amino]carbonyl}amino)-1-[(methyloxy)methyl]ethyl phenylcarbamate

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