3,5-di-O-benzoyl-2-deoxy-2-fluoro-4-C-methyl-α,β-D-arabinofuranosyl bromide

Base Information

Chemical Name:3,5-di-O-benzoyl-2-deoxy-2-fluoro-4-C-methyl-α,β-D-arabinofuranosyl bromide
CAS No.:1203477-23-9
Molecular Formula:C₂₀H₁₈BrFO₅
Molecular Weight:437.262
Hs Code.:

Synonyms:3,5-di-O-benzoyl-2-deoxy-2-fluoro-4-C-methyl-α,β-D-arabinofuranosyl bromide

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Chemical Property of 3,5-di-O-benzoyl-2-deoxy-2-fluoro-4-C-methyl-α,β-D-arabinofuranosyl bromide

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Technology Process of 3,5-di-O-benzoyl-2-deoxy-2-fluoro-4-C-methyl-α,β-D-arabinofuranosyl bromide

There total 3 articles about 3,5-di-O-benzoyl-2-deoxy-2-fluoro-4-C-methyl-α,β-D-arabinofuranosyl bromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1203477-22-8
1-O-acetyl-3,5-di-O-benzoyl-2-deoxy-2-fluoro-4-C-methyl-D-arabinofuranose

: 1203477-23-9
3,5-di-O-benzoyl-2-deoxy-2-fluoro-4-C-methyl-α,β-D-arabinofuranosyl bromide

Guidance literature:: 1-O-acetyl-3,5-di-O-benzoyl-2-deoxy-2-fluoro-4-C-methyl-D-arabinofuranose; With magnesium sulfate; In dichloromethane; for 1.5h;

With hydrogen bromide; acetic anhydride; In dichloromethane;

Reference yield:

: 1-O-acetyl-3,5-di-O-benzoyl-2-deoxy-2-fluoro-4-C-methyl-α,β-D-arabinofuranose

: 1203477-23-9
3,5-di-O-benzoyl-2-deoxy-2-fluoro-4-C-methyl-α,β-D-arabinofuranosyl bromide

Guidance literature:: With hydrogen bromide; In dichloromethane; acetic acid; at 5 ℃; Inert atmosphere;
DOI:10.1080/15257770903091946

Reference yield:

: 1203477-19-3
methyl 3,5-di-O-benzoyl-2-deoxy-2-fluoro-4-C-methyl-β-D-arabinofuranoside

: 1203477-23-9
3,5-di-O-benzoyl-2-deoxy-2-fluoro-4-C-methyl-α,β-D-arabinofuranosyl bromide

Guidance literature:: Multi-step reaction with 2 steps

1: acetic acid; sulfuric acid / dichloromethane / 20 °C / Cooling with ice

2: acetic acid; hydrogen bromide / dichloromethane / 25 °C

With sulfuric acid; hydrogen bromide; acetic acid; In dichloromethane;