Sn2(μ-Cl)2(N(SiMe3)(2,6-diisopropylphenyl))2

Base Information

Chemical Name:Sn2(μ-Cl)2(N(SiMe3)(2,6-diisopropylphenyl))2
CAS No.:891638-22-5
Molecular Formula:C₃₀H₅₂Cl₂N₂Si₂Sn₂
Molecular Weight:805.253
Hs Code.:

Synonyms:Sn2(μ-Cl)2(N(SiMe3)(2,6-diisopropylphenyl))2

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Chemical Property of Sn2(μ-Cl)2(N(SiMe3)(2,6-diisopropylphenyl))2

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Technology Process of Sn2(μ-Cl)2(N(SiMe3)(2,6-diisopropylphenyl))2

There total 1 articles about Sn2(μ-Cl)2(N(SiMe3)(2,6-diisopropylphenyl))2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: bis(N-trimethylsilyl-N-2,6-diisopropylphenylamido)tin(II)

: tin(ll) chloride

: 891638-22-5
Sn2(μ-Cl)2(N(SiMe3)(2,6-diisopropylphenyl))2

Guidance literature:: In diethyl ether;
DOI:10.1002/anie.200600292

Reference yield: 54.0%

: 891638-22-5
Sn2(μ-Cl)2(N(SiMe3)(2,6-diisopropylphenyl))2

: 56174-66-4
2-(N,N-dimethylaminomethyl)phenyllithium

: 1257639-45-4
(2-((CH₃)2NCH₂)C₆H₄)Sn(N(SiMe₃)(2,6-diisopropylphenyl))

Guidance literature:: In diethyl ether; byproducts: LiCl; (Ar, Schlenk technique); addn. of ethereal suspn. of lithium deriv. to ethereal soln. of tin compd. at -30°C for 20 min, slow warming to room temp., stirring overnight; evapn., extn. (hexane), evapn., elem. anal.;
DOI:10.1016/j.jorganchem.2010.08.013

Reference yield:

: 891638-22-5
Sn2(μ-Cl)2(N(SiMe3)(2,6-diisopropylphenyl))2

: [(tin(II))15(N(2,6-iPr₂C₆H₃)(SiMe₃))6] C₉₀H₁₅₆N₆Si₆Sn₁₅, trigonal, R₃-

Guidance literature:: With KC₈; In diethyl ether; exclusion of air and moisture; KC8 (0.81 mmol) added with stirring to soln. of (Sn(N(C6H3(CH3CHCH3)2)(Si(CH3)3))Cl)2 (0.55 mmol) at -30°C, mixt. stirred for 5 h; filtered, concd., toluene added, stored at -27°C; when crystals of unreacted amidotin(II) chloride pptd. soln. decanted, concd., stored at room temp.;
DOI:10.1002/anie.200600292