allyl (methyl 2-O-benzoyl-3-O-benzyl-β-D-glucopyranosyluronate-(1->3)-4-O-acetyl-6-O-benzyl-2-deoxy-2-trichloroacetamido-β-D-glucopyranosyl)-(1->4)-(methyl 2-O-benzoyl-3-O-benzyl-β-D-glucopyranosyluronate)-(1->3)-4-O-acetyl-6-O-benzyl-2-deoxy-2-trichloroacetamido-β-D-glucopyranoside

Base Information

• Chemical Name: allyl (methyl 2-O-benzoyl-3-O-benzyl-β-D-glucopyranosyluronate-(1->3)-4-O-acetyl-6-O-benzyl-2-deoxy-2-trichloroacetamido-β-D-glucopyranosyl)-(1->4)-(methyl 2-O-benzoyl-3-O-benzyl-β-D-glucopyranosyluronate)-(1->3)-4-O-acetyl-6-O-benzyl-2-deoxy-2-trichloroacetamido-β-D-glucopyranoside
• CAS No.: 1260246-84-1
• Molecular Formula: C₇₉H₈₂Cl₆N₂O₂₇
• Molecular Weight: 1704.24

Synonyms:allyl (methyl 2-O-benzoyl-3-O-benzyl-β-D-glucopyranosyluronate-(1->3)-4-O-acetyl-6-O-benzyl-2-deoxy-2-trichloroacetamido-β-D-glucopyranosyl)-(1->4)-(methyl 2-O-benzoyl-3-O-benzyl-β-D-glucopyranosyluronate)-(1->3)-4-O-acetyl-6-O-benzyl-2-deoxy-2-trichloroacetamido-β-D-glucopyranoside

Chemical Property of allyl (methyl 2-O-benzoyl-3-O-benzyl-β-D-glucopyranosyluronate-(1->3)-4-O-acetyl-6-O-benzyl-2-deoxy-2-trichloroacetamido-β-D-glucopyranosyl)-(1->4)-(methyl 2-O-benzoyl-3-O-benzyl-β-D-glucopyranosyluronate)-(1->3)-4-O-acetyl-6-O-benzyl-2-deoxy-2-trichloroacetamido-β-D-glucopyranoside

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Technology Process of allyl (methyl 2-O-benzoyl-3-O-benzyl-β-D-glucopyranosyluronate-(1->3)-4-O-acetyl-6-O-benzyl-2-deoxy-2-trichloroacetamido-β-D-glucopyranosyl)-(1->4)-(methyl 2-O-benzoyl-3-O-benzyl-β-D-glucopyranosyluronate)-(1->3)-4-O-acetyl-6-O-benzyl-2-deoxy-2-trichloroacetamido-β-D-glucopyranoside

There total 1 articles about allyl (methyl 2-O-benzoyl-3-O-benzyl-β-D-glucopyranosyluronate-(1->3)-4-O-acetyl-6-O-benzyl-2-deoxy-2-trichloroacetamido-β-D-glucopyranosyl)-(1->4)-(methyl 2-O-benzoyl-3-O-benzyl-β-D-glucopyranosyluronate)-(1->3)-4-O-acetyl-6-O-benzyl-2-deoxy-2-trichloroacetamido-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

allyl (methyl 2-O-benzoyl-3-O-benzyl-4-O-levulinoyl-β-D-glucopyranosyluronate-(1->3)-4-O-acetyl-6-O-benzyl-2-deoxy-2-trichloroacetamido-β-D-glucopyranosyl)-(1->4)-(methyl 2-O-benzoyl-3-O-benzyl-β-D-glucopyranosyluronate)-(1->3)-4-O-acetyl-6-O-benzyl-2-deoxy-2-trichloroacetamido-β-D-glucopyranoside (1260246-83-0) → allyl (methyl 2-O-benzoyl-3-O-benzyl-β-D-glucopyranosyluronate-(1->3)-4-O-acetyl-6-O-benzyl-2-deoxy-2-trichloroacetamido-β-D-glucopyranosyl)-(1->4)-(methyl 2-O-benzoyl-3-O-benzyl-β-D-glucopyranosyluronate)-(1->3)-4-O-acetyl-6-O-benzyl-2-deoxy-2-trichloroacetamido-β-D-glucopyranoside (1260246-84-1)

Guidance literature:

With hydrazinium monoacetate; In methanol; dichloromethane; at 20 ℃; for 2h; Inert atmosphere;

DOI:10.1002/adsc.201000008

Reference yield: 49.0%

methyl 2-O-benzoyl-3-O-benzyl-4-O-levulinoyl-β-D-glucopyranosyluronate-(1->3)-4-O-acetyl-6-O-benzyl-2-deoxy-2-trichloroacetamido-α-D-glucopyranosyl-trichloroacetimidate (1260246-81-8) + allyl (methyl 2-O-benzoyl-3-O-benzyl-β-D-glucopyranosyluronate-(1->3)-4-O-acetyl-6-O-benzyl-2-deoxy-2-trichloroacetamido-β-D-glucopyranosyl)-(1->4)-(methyl 2-O-benzoyl-3-O-benzyl-β-D-glucopyranosyluronate)-(1->3)-4-O-acetyl-6-O-benzyl-2-deoxy-2-trichloroacetamido-β-D-glucopyranoside (1260246-84-1) → allyl (methyl 2-O-benzoyl-3-O-benzyl-4-O-levulinoyl-β-D-glucopyranosyluronate-(1->3)-4-O-acetyl-6-O-benzyl-2-deoxy-2-trichloroacetamido-β-D-glucopyranosyl)-(1->4)-(methyl 2-O-benzoyl-3-O-benzyl-β-D-glucopyranosyluronate-(1->3)-4-O-acetyl-6-O-benzyl-2-deoxy-2-trichloroacetamido-β-D-glucopyranosyl)-(1->4)-(methyl 2-O-benzoyl-3-O-benzyl-β-D-glucopyranosyluronate)-(1->3)-4-O-acetyl-6-O-benzyl-2-deoxy-2-trichloroacetamido-β-D-glucopyranoside (1260246-85-2)

Guidance literature:

With trimethylsilyl trifluoromethanesulfonate; In dichloromethane; at 0 ℃; for 1.5h; Inert atmosphere;

DOI:10.1002/adsc.201000008

Reference yield: 15.0%

allyl (methyl 2-O-benzoyl-3-O-benzyl-β-D-glucopyranosyluronate-(1->3)-4-O-acetyl-6-O-benzyl-2-deoxy-2-trichloroacetamido-β-D-glucopyranosyl)-(1->4)-(methyl 2-O-benzoyl-3-O-benzyl-β-D-glucopyranosyluronate)-(1->3)-4-O-acetyl-6-O-benzyl-2-deoxy-2-trichloroacetamido-β-D-glucopyranoside (1260246-84-1) → allyl (methyl 2-O-benzoyl-3-O-benzyl-β-D-glucopyranosyluronate-(1->3)-4-O-acetyl-6-O-benzyl-2-deoxy-2-acetamido-β-D-glucopyranosyl)-(1->4)-(methyl 2-O-benzoyl-3-O-benzyl-β-D-glucopyranosyluronate)-(1->3)-4-O-acetyl-6-O-benzyl-2-deoxy-2-acetamido-β-D-glucopyranoside (1260246-88-5)

Guidance literature:

With acetic acid; zinc; In 1,4-dioxane; at 20 ℃; Inert atmosphere;

DOI:10.1002/adsc.201000008

upstream raw materials:

allyl (methyl 2-O-benzoyl-3-O-benzyl-4-O-levulinoyl-β-D-glucopyranosyluronate-(1->3)-4-O-acetyl-6-O-benzyl-2-deoxy-2-trichloroacetamido-β-D-glucopyranosyl)-(1->4)-(methyl 2-O-benzoyl-3-O-benzyl-β-D-glucopyranosyluronate)-(1->3)-4-O-acetyl-6-O-benzyl-2-deoxy-2-trichloroacetamido-β-D-glucopyranoside

Downstream raw materials:

allyl (methyl 2-O-benzoyl-3-O-benzyl-4-O-levulinoyl-β-D-glucopyranosyluronate-(1->3)-4-O-acetyl-6-O-benzyl-2-deoxy-2-trichloroacetamido-β-D-glucopyranosyl)-(1->4)-(methyl 2-O-benzoyl-3-O-benzyl-β-D-glucopyranosyluronate-(1->3)-4-O-acetyl-6-O-benzyl-2-deoxy-2-trichloroacetamido-β-D-glucopyranosyl)-(1->4)-(methyl 2-O-benzoyl-3-O-benzyl-β-D-glucopyranosyluronate)-(1->3)-4-O-acetyl-6-O-benzyl-2-deoxy-2-trichloroacetamido-β-D-glucopyranoside

allyl (methyl 2-O-benzoyl-3-O-benzyl-β-D-glucopyranosyluronate-(1->3)-4-O-acetyl-6-O-benzyl-2-deoxy-2-acetamido-β-D-glucopyranosyl)-(1->4)-(methyl 2-O-benzoyl-3-O-benzyl-β-D-glucopyranosyluronate)-(1->3)-4-O-acetyl-6-O-benzyl-2-deoxy-2-acetamido-β-D-glucopyranoside

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