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Technology Process of C12H7N2(C6H5)2C3(CH3)4N2O2

C12H7N2(C6H5)2C3(CH3)4N2O2

Base Information
  • Chemical Name:C12H7N2(C6H5)2C3(CH3)4N2O2
  • CAS No.:653593-26-1
  • Molecular Formula:C31H29N4O2
  • Molecular Weight:489.597
  • Hs Code.:
C<sub>12</sub>H<sub>7</sub>N<sub>2</sub>(C<sub>6</sub>H<sub>5</sub>)2C<sub>3</sub>(CH<sub>3</sub>)4N<sub>2</sub>O<sub>2</sub>

Synonyms:C12H7N2(C6H5)2C3(CH3)4N2O2

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Chemical Property of C12H7N2(C6H5)2C3(CH3)4N2O2
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Technology Process of C12H7N2(C6H5)2C3(CH3)4N2O2

There total 2 articles about C12H7N2(C6H5)2C3(CH3)4N2O2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-(5,10-diphenyl-5,10-dihydro-phenazin-2-yl)-4,4,5,5-tetramethyl-imidazolidine-1,3-diol
653593-31-8

2-(5,10-diphenyl-5,10-dihydro-phenazin-2-yl)-4,4,5,5-tetramethyl-imidazolidine-1,3-diol

C<sub>12</sub>H<sub>7</sub>N<sub>2</sub>(C<sub>6</sub>H<sub>5</sub>)2C<sub>3</sub>(CH<sub>3</sub>)4N<sub>2</sub>O<sub>2</sub>
653593-26-1

C12H7N2(C6H5)2C3(CH3)4N2O2

Guidance literature:
With silver(l) oxide; In dichloromethane;
DOI:10.1021/ja0367748

Reference yield:

2-dimethoxymethyl-5,10-diphenyl-5,10-dihydro-phenazine

2-dimethoxymethyl-5,10-diphenyl-5,10-dihydro-phenazine

C<sub>12</sub>H<sub>7</sub>N<sub>2</sub>(C<sub>6</sub>H<sub>5</sub>)2C<sub>3</sub>(CH<sub>3</sub>)4N<sub>2</sub>O<sub>2</sub>
653593-26-1

C12H7N2(C6H5)2C3(CH3)4N2O2

Guidance literature:
Multi-step reaction with 2 steps
1: pyridinium tosylate / methanol
2: Ag2O / CH2Cl2
With pyridinium p-toluenesulfonate; silver(l) oxide; In methanol; dichloromethane;
DOI:10.1021/ja0367748

Reference yield: 57.0%

thianthreniumyl tetrabromoferrate(III)

thianthreniumyl tetrabromoferrate(III)

C<sub>12</sub>H<sub>7</sub>N<sub>2</sub>(C<sub>6</sub>H<sub>5</sub>)2C<sub>3</sub>(CH<sub>3</sub>)4N<sub>2</sub>O<sub>2</sub>
653593-26-1

C12H7N2(C6H5)2C3(CH3)4N2O2

C<sub>12</sub>H<sub>7</sub>N<sub>2</sub>(C<sub>6</sub>H<sub>5</sub>)2C<sub>3</sub>(CH<sub>3</sub>)4N<sub>2</sub>O<sub>2</sub><sup>(1+)</sup>*FeBr<sub>4</sub><sup>(1-)</sup>=C<sub>12</sub>H<sub>7</sub>N<sub>2</sub>(C<sub>6</sub>H<sub>5</sub>)2C<sub>3</sub>(CH<sub>3</sub>)4N<sub>2</sub>O<sub>2</sub>FeBr<sub>4</sub>

C12H7N2(C6H5)2C3(CH3)4N2O2(1+)*FeBr4(1-)=C12H7N2(C6H5)2C3(CH3)4N2O2FeBr4

Guidance literature:
In dichloromethane; acetonitrile; in glovebox; soln. of thianthreniumyl-FeBr4 in CH3CN added to soln. of phenazine-compd. in CH2Cl2 at room temp., mixt. was stirred for 30 min; soln. filtered, filtrate evapd. under vac., residue dissolved in CH2Cl2,excess of Et2O added, solid sepd. and dissolved in ClCH2CH2Cl in small flask, flask placed in larger one contg. pentane, covered system stored at room temp. for 3 d; elem. anal.;
upstream raw materials:

2-(5,10-diphenyl-5,10-dihydro-phenazin-2-yl)-4,4,5,5-tetramethyl-imidazolidine-1,3-diol

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