[2-(Trityl-amino)-acetylamino]-acetic acid (3R,4aR,5S,6S,6aS,10S,10aR,10bS)-5-acetoxy-10,10b-dihydroxy-3,4a,7,7,10a-pentamethyl-1-oxo-3-vinyl-dodecahydro-benzo[f]chromen-6-yl ester

Base Information

Chemical Name:[2-(Trityl-amino)-acetylamino]-acetic acid (3R,4aR,5S,6S,6aS,10S,10aR,10bS)-5-acetoxy-10,10b-dihydroxy-3,4a,7,7,10a-pentamethyl-1-oxo-3-vinyl-dodecahydro-benzo[f]chromen-6-yl ester
CAS No.:928045-96-9
Molecular Formula:C₄₅H₅₄N₂O₉
Molecular Weight:766.932
Hs Code.:

[2-(Trityl-amino)-acetylamino]-acetic acid (3R,4aR,5S,6S,6aS,10S,10aR,10bS)-5-acetoxy-10,10b-dihydroxy-3,4a,7,7,10a-pentamethyl-1-oxo-3-vinyl-dodecahydro-benzo[f]chromen-6-yl ester

Synonyms:[2-(Trityl-amino)-acetylamino]-acetic acid (3R,4aR,5S,6S,6aS,10S,10aR,10bS)-5-acetoxy-10,10b-dihydroxy-3,4a,7,7,10a-pentamethyl-1-oxo-3-vinyl-dodecahydro-benzo[f]chromen-6-yl ester

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Chemical Property of [2-(Trityl-amino)-acetylamino]-acetic acid (3R,4aR,5S,6S,6aS,10S,10aR,10bS)-5-acetoxy-10,10b-dihydroxy-3,4a,7,7,10a-pentamethyl-1-oxo-3-vinyl-dodecahydro-benzo[f]chromen-6-yl ester

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Technology Process of [2-(Trityl-amino)-acetylamino]-acetic acid (3R,4aR,5S,6S,6aS,10S,10aR,10bS)-5-acetoxy-10,10b-dihydroxy-3,4a,7,7,10a-pentamethyl-1-oxo-3-vinyl-dodecahydro-benzo[f]chromen-6-yl ester

There total 4 articles about [2-(Trityl-amino)-acetylamino]-acetic acid (3R,4aR,5S,6S,6aS,10S,10aR,10bS)-5-acetoxy-10,10b-dihydroxy-3,4a,7,7,10a-pentamethyl-1-oxo-3-vinyl-dodecahydro-benzo[f]chromen-6-yl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 928045-94-7
[2-(Trityl-amino)-acetylamino]-acetic acid (3R,4aR,5S,6S,6aS,10S,10aR,10bS)-10-(tert-butyl-dimethyl-silanyloxy)-5,10b-dihydroxy-3,4a,7,7,10a-pentamethyl-1-oxo-3-vinyl-dodecahydro-benzo[f]chromen-6-yl ester

: 928045-96-9
[2-(Trityl-amino)-acetylamino]-acetic acid (3R,4aR,5S,6S,6aS,10S,10aR,10bS)-5-acetoxy-10,10b-dihydroxy-3,4a,7,7,10a-pentamethyl-1-oxo-3-vinyl-dodecahydro-benzo[f]chromen-6-yl ester

Guidance literature:: With 4 A molecular sieve; tetrabutyl ammonium fluoride; In tetrahydrofuran; at 20 ℃; for 0.166667h;

Reference yield:

: 928045-93-6
[2-(Trityl-amino)-acetylamino]-acetic acid (3R,4aR,5S,6S,6aS,10S,10aR,10bS)-10-(tert-butyl-dimethyl-silanyloxy)-6,10b-dihydroxy-3,4a,7,7,10a-pentamethyl-1-oxo-3-vinyl-dodecahydro-benzo[f]chromen-5-yl ester

: 928045-96-9
[2-(Trityl-amino)-acetylamino]-acetic acid (3R,4aR,5S,6S,6aS,10S,10aR,10bS)-5-acetoxy-10,10b-dihydroxy-3,4a,7,7,10a-pentamethyl-1-oxo-3-vinyl-dodecahydro-benzo[f]chromen-6-yl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 70.2 percent / Na₂CO₃ / acetonitrile; dimethylformamide; H₂O / 3 h / 20 °C

2: 92 percent / (nBu)4NF; molecular sieves 4 Angstroem / tetrahydrofuran / 0.17 h / 20 °C

With 4 A molecular sieve; tetrabutyl ammonium fluoride; sodium carbonate; In tetrahydrofuran; water; N,N-dimethyl-formamide; acetonitrile;

Reference yield:

: 5893-07-2
N-tritylglycylglycine

: 928045-96-9
[2-(Trityl-amino)-acetylamino]-acetic acid (3R,4aR,5S,6S,6aS,10S,10aR,10bS)-5-acetoxy-10,10b-dihydroxy-3,4a,7,7,10a-pentamethyl-1-oxo-3-vinyl-dodecahydro-benzo[f]chromen-6-yl ester

Guidance literature:: Multi-step reaction with 3 steps

1: DCC; DMAP / ethyl acetate; dimethylformamide / 20 °C

2: 70.2 percent / Na₂CO₃ / acetonitrile; dimethylformamide; H₂O / 3 h / 20 °C

3: 92 percent / (nBu)4NF; molecular sieves 4 Angstroem / tetrahydrofuran / 0.17 h / 20 °C

With dmap; 4 A molecular sieve; tetrabutyl ammonium fluoride; sodium carbonate; dicyclohexyl-carbodiimide; In tetrahydrofuran; water; ethyl acetate; N,N-dimethyl-formamide; acetonitrile;