C₂₀H₂₆F₄N₂O₄

Base Information

Chemical Name:C₂₀H₂₆F₄N₂O₄
CAS No.:1310839-68-9
Molecular Formula:C₂₀H₂₆F₄N₂O₄
Molecular Weight:434.431
Hs Code.:

C<sub>20</sub>H<sub>26</sub>F<sub>4</sub>N<sub>2</sub>O<sub>4</sub>

Synonyms:C₂₀H₂₆F₄N₂O₄

Suppliers and Price of C₂₀H₂₆F₄N₂O₄

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₀H₂₆F₄N₂O₄

Chemical Property:

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Technology Process of C₂₀H₂₆F₄N₂O₄

There total 8 articles about C₂₀H₂₆F₄N₂O₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 24424-99-5
di-tert-butyl dicarbonate

: C₁₅H₁₈F₄N₂O₂

: 1310839-68-9
C₂₀H₂₆F₄N₂O₄

Guidance literature:: In tetrahydrofuran; at 20 - 70 ℃; for 14h;

Reference yield:

: 4117-10-6
6-hepten-1-ol

: 1310839-68-9
C₂₀H₂₆F₄N₂O₄

Guidance literature:: Multi-step reaction with 8 steps

1.1: 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione / ethyl acetate / 3 h / 20 °C / Reflux

1.2: 1.5 h / 20 °C

2.1: sodium hypochlorite / dichloromethane; water / 0.5 h / 20 °C

3.1: n-butyllithium / toluene; hexane; tetrahydrofuran / 0.5 h / -70 °C / Inert atmosphere

3.2: 0.42 h / -70 °C / Inert atmosphere

3.3: 1.25 h / -70 °C / Inert atmosphere

4.1: nitric acid; sulfuric acid / 1 h / Cooling with ice

5.1: ammonium chloride; iron / ethanol; water / 2 h / 20 - 45 °C

6.1: triethylamine / methanol / 4 h / 20 °C

7.1: hydrogen / 5% rhodium-on-charcoal / ethanol / 23 h / 20 °C

8.1: tetrahydrofuran / 14 h / 20 - 70 °C

With sodium hypochlorite; n-butyllithium; sulfuric acid; hydrogen; nitric acid; iron; ammonium chloride; triethylamine; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione; 5% rhodium-on-charcoal; In tetrahydrofuran; methanol; ethanol; hexane; dichloromethane; water; ethyl acetate; toluene;

Reference yield:

: 3,3a,4,5,6,7-hexahydrobenzo[c]isoxazole

: 1310839-68-9
C₂₀H₂₆F₄N₂O₄

Guidance literature:: Multi-step reaction with 6 steps

1.1: n-butyllithium / toluene; hexane; tetrahydrofuran / 0.5 h / -70 °C / Inert atmosphere

1.2: 0.42 h / -70 °C / Inert atmosphere

1.3: 1.25 h / -70 °C / Inert atmosphere

2.1: nitric acid; sulfuric acid / 1 h / Cooling with ice

3.1: ammonium chloride; iron / ethanol; water / 2 h / 20 - 45 °C

4.1: triethylamine / methanol / 4 h / 20 °C

5.1: hydrogen / 5% rhodium-on-charcoal / ethanol / 23 h / 20 °C

6.1: tetrahydrofuran / 14 h / 20 - 70 °C

With n-butyllithium; sulfuric acid; hydrogen; nitric acid; iron; ammonium chloride; triethylamine; 5% rhodium-on-charcoal; In tetrahydrofuran; methanol; ethanol; hexane; water; toluene;