C₃₃H₃₈O₆S

Base Information

Chemical Name:C₃₃H₃₈O₆S
CAS No.:187458-50-0
Molecular Formula:C₃₃H₃₈O₆S
Molecular Weight:562.727
Hs Code.:

C<sub>33</sub>H<sub>38</sub>O<sub>6</sub>S

Synonyms:C₃₃H₃₈O₆S

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Chemical Property of C₃₃H₃₈O₆S

Chemical Property:

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Technology Process of C₃₃H₃₈O₆S

There total 24 articles about C₃₃H₃₈O₆S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 1005-56-7
phenylcarbonochloridothioate

: 187458-49-7
C₂₆H₃₄O₅

: 187458-50-0
C₃₃H₃₈O₆S

Guidance literature:: With pyridine; dmap; In dichloromethane; for 1h; Ambient temperature;
DOI:10.1021/jo961993f

Reference yield:

: 498-60-2
furan-3-carboxaldehyde

: 187458-50-0
C₃₃H₃₈O₆S

Guidance literature:: Multi-step reaction with 12 steps

2: 96 percent / carbon tetrabromide, Ph₃P / CH₂Cl₂ / 0.33 h / 0 °C

3: 90 percent / hexamethylphosphoric acid triamide / 2 h / 15 °C

4: 1) MeMgSnBu₃, CuCN, 2) I₂, Na₂CO₃ / 1) THF, 0 deg C, 20 min, 2) 0 deg C

5: 95 percent / tetrabutylammonium chloride, K₂CO₃, Pd(OAc)2 / dimethylformamide / 3 h / Ambient temperature

6: 88 percent / DIBAL-H / CH₂Cl₂; hexane / 0.33 h / -78 °C

7: 95 percent / BaMnO₄ / CH₂Cl₂ / 6 h / Ambient temperature

8: PPh₃ / CH₂Cl₂ / 0 °C

9: LDA / tetrahydrofuran / 0.5 h / 0 °C

10: 1) MeMgSnBu₃, CuCN, 2) I₂, Na₂CO₃ / 1) THF, hexane, -20 deg C, 20 min, 2) CH₂Cl₂, 0 deg C

11: 60 percent / CrCl₂, NiCl₂ / dimethylsulfoxide / 18 h / Ambient temperature

12: 89 percent / DMAP, pyridine / CH₂Cl₂ / 1 h / Ambient temperature

With pyridine; chromium dichloride; dmap; palladium diacetate; barium permanganate; methylmagnesium tributylstannane; carbon tetrabromide; tetrabutyl-ammonium chloride; iodine; diisobutylaluminium hydride; sodium carbonate; potassium carbonate; triphenylphosphine; nickel dichloride; lithium diisopropyl amide; In tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide; hexane; dichloromethane; dimethyl sulfoxide; N,N-dimethyl-formamide;
DOI:10.1021/jo961993f

Reference yield:

: 27205-80-7
4-methoxy-3-methyl-2(5H)-furanone

: 187458-50-0
C₃₃H₃₈O₆S

Guidance literature:: Multi-step reaction with 7 steps

1: LDA / tetrahydrofuran; hexamethylphosphoric acid triamide / 0.33 h / -78 °C

2: Et₃N, DMAP / CH₂Cl₂ / 0.08 h / 0 °C

3: DBU / benzene / 0.17 h / Ambient temperature

4: 62 percent / Bu₄NF / tetrahydrofuran / 0.5 h

5: 68 percent / PCC / CH₂Cl₂ / 1 h / Ambient temperature

6: 60 percent / CrCl₂, NiCl₂ / dimethylsulfoxide / 18 h / Ambient temperature

7: 89 percent / DMAP, pyridine / CH₂Cl₂ / 1 h / Ambient temperature

With pyridine; chromium dichloride; dmap; tetrabutyl ammonium fluoride; 1,8-diazabicyclo[5.4.0]undec-7-ene; triethylamine; pyridinium chlorochromate; nickel dichloride; lithium diisopropyl amide; In tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide; dichloromethane; dimethyl sulfoxide; benzene;
DOI:10.1021/jo961993f