C₂₃H₂₈Cl₂N₄O

Base Information

Chemical Name:C₂₃H₂₈Cl₂N₄O
CAS No.:1092069-74-3
Molecular Formula:C₂₃H₂₈Cl₂N₄O
Molecular Weight:447.408
Hs Code.:

C<sub>23</sub>H<sub>28</sub>Cl<sub>2</sub>N<sub>4</sub>O

Synonyms:C₂₃H₂₈Cl₂N₄O

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Chemical Property of C₂₃H₂₈Cl₂N₄O

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Technology Process of C₂₃H₂₈Cl₂N₄O

There total 8 articles about C₂₃H₂₈Cl₂N₄O which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 58.0%

: 1092069-73-2
C₂₃H₂₆Cl₂N₄O₃

: 1092069-74-3
C₂₃H₂₈Cl₂N₄O

Guidance literature:: With hydrazine; Raney Nickel; In methanol; water; for 0.166667h; Heating / reflux;

Reference yield:

: 1092170-37-0
C₁₄H₁₇Cl₂NO₂

: 1092069-74-3
C₂₃H₂₈Cl₂N₄O

Guidance literature:: Multi-step reaction with 4 steps

1.1: hydrogenchloride / diethyl ether

2.1: lithium hydroxide; water / methanol / 0.33 h / Heating / reflux

2.2: 0.08 h / Heating / reflux

3.1: diethyl cyanophosphonate; triethylamine / dichloromethane / 0.17 h / 20 °C

3.2: 5 h / 20 °C

4.1: hydrazine / Raney Nickel .(R). / methanol; water / 0.17 h / Heating / reflux

With hydrogenchloride; lithium hydroxide; diethyl cyanophosphonate; water; triethylamine; hydrazine; Raney Nickel; In methanol; diethyl ether; dichloromethane; water;

Reference yield:

: 185153-53-1
2,6-dichloro-4-methyl-benzeneacetic acid methyl ester

: 1092069-74-3
C₂₃H₂₈Cl₂N₄O

Guidance literature:: Multi-step reaction with 6 steps

1.1: N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile) / tetrachloromethane / 10 h / Heating / reflux

2.1: 0.08 h / 90 - 100 °C

3.1: hydrogenchloride / diethyl ether

4.1: lithium hydroxide; water / methanol / 0.33 h / Heating / reflux

4.2: 0.08 h / Heating / reflux

5.1: diethyl cyanophosphonate; triethylamine / dichloromethane / 0.17 h / 20 °C

5.2: 5 h / 20 °C

6.1: hydrazine / Raney Nickel .(R). / methanol; water / 0.17 h / Heating / reflux

With hydrogenchloride; lithium hydroxide; N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile); diethyl cyanophosphonate; water; triethylamine; hydrazine; Raney Nickel; In methanol; tetrachloromethane; diethyl ether; dichloromethane; water;