p-Octyloxybenzyl alcohol

Base Information

• Chemical Name: p-Octyloxybenzyl alcohol
• CAS No.: 67698-68-4
• Molecular Formula: C15H24O2
• Molecular Weight: 236.354
• Mol file: 67698-68-4.mol

Synonyms:p-octyloxyphenylmethanol;p-Octyloxybenzyl alcohol;4-Octyloxybenzyl alcohol;p-n-octyloxybenzyl alcohol;

Chemical Property of p-Octyloxybenzyl alcohol

Chemical Property:

• Vapor Pressure: 1.05E-05mmHg at 25°C
• Boiling Point: 356.6°C at 760 mmHg
• Flash Point: 145.4°C
• PSA: 29.46000
• Density: 0.973g/cm³
• LogP: 3.91820

Purity/Quality:

90% ^*data from raw suppliers

p-Octyloxybenzyl alcohol ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of p-Octyloxybenzyl alcohol

There total 12 articles about p-Octyloxybenzyl alcohol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

methyl 4-(octyloxy)benzoate (62435-37-4) → p-n-octyloxybenzyl alcohol (67698-68-4)

Guidance literature:

With lithium aluminium tetrahydride; In tetrahydrofuran; a) RT, 1 h, b) reflux, 0.5 h;

DOI:10.1002/jccs.199700014

Reference yield: 94.0%

1-bromo-octane (111-83-1) + 4-hydroxy-benzaldehyde (123-08-0,65581-83-1) → p-n-octyloxybenzyl alcohol (67698-68-4)

Guidance literature:

4-hydroxy-benzaldehyde; With potassium carbonate; In N,N-dimethyl-formamide; at 90 ℃; for 1h;

1-bromo-octane; With potassium carbonate; In N,N-dimethyl-formamide; at 20 ℃; for 3h;

With methanol; sodium tetrahydroborate; for 1.5h;

DOI:10.1016/j.carres.2005.07.011

Reference yield: 82.0%

4-octyloxy-benzoic acid ethyl ester (72885-31-5) → p-n-octyloxybenzyl alcohol (67698-68-4)

Guidance literature:

With sodium bis(2-methoxyethoxy)aluminium dihydride; In toluene; at 0 - 21 ℃; for 16.5h; Inert atmosphere; Sealed tube;

DOI:10.1039/c5ob00621j

upstream raw materials:

methyl 4-(octyloxy)benzoate

1-bromo-octane

4-hydroxy-benzaldehyde

4-octyloxybenzaldehyde

Downstream raw materials:

4-octyloxybenzaldehyde

p-octyloxyphenylmethanethiol

C₁₈H₂₈O₃