2-(2-benzyloxy-acetylamino)-3-(4-hydroxy-phenyl)-propionic acid methoxy carbonyl methyl ester

Base Information

• Chemical Name: 2-(2-benzyloxy-acetylamino)-3-(4-hydroxy-phenyl)-propionic acid methoxy carbonyl methyl ester
• CAS No.: 934740-86-0
• Molecular Formula: C₂₁H₂₃NO₇
• Molecular Weight: 401.416

Synonyms:2-(2-benzyloxy-acetylamino)-3-(4-hydroxy-phenyl)-propionic acid methoxy carbonyl methyl ester

Chemical Property of 2-(2-benzyloxy-acetylamino)-3-(4-hydroxy-phenyl)-propionic acid methoxy carbonyl methyl ester

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Technology Process of 2-(2-benzyloxy-acetylamino)-3-(4-hydroxy-phenyl)-propionic acid methoxy carbonyl methyl ester

There total 1 articles about 2-(2-benzyloxy-acetylamino)-3-(4-hydroxy-phenyl)-propionic acid methoxy carbonyl methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 33.3%

2-(2-benzyloxy-acetylamino)-3-(4-hydroxy-phenyl)-propionic acid (934740-85-9) + methyl chloroacetate (96-34-4) → 2-(2-benzyloxy-acetylamino)-3-(4-hydroxy-phenyl)-propionic acid methoxy carbonyl methyl ester (934740-86-0)

Guidance literature:

With triethylamine; In acetone; for 16h; Heating / reflux;

Reference yield: 64.5%

2-(2-benzyloxy-acetylamino)-3-(4-hydroxy-phenyl)-propionic acid methoxy carbonyl methyl ester (934740-86-0) + methyl chloroacetate (96-34-4) → 2-(2-benzyloxy-acetylamino)-3-(4-methoxycarbonylmethoxy-phenyl)-propionic acid 2-methoxycarbonyl-ethyl ester (934740-87-1)

Guidance literature:

With potassium carbonate; sodium iodide; In acetone; for 16h; Heating / reflux;

Reference yield: 52.5%

2-(2-benzyloxy-acetylamino)-3-(4-hydroxy-phenyl)-propionic acid methoxy carbonyl methyl ester (934740-86-0) + Benzyloxyacetyl chloride (19810-31-2) → 3-[4-(2-benzyloxy-acetoxy)-phenyl]-2-(2-benzyloxy-acetylamino)-propionic acid methoxycarbonylmethyl ester (934740-90-6)

Guidance literature:

With triethylamine; In acetone; for 16h;

upstream raw materials:

2-(2-benzyloxy-acetylamino)-3-(4-hydroxy-phenyl)-propionic acid

methyl chloroacetate

Downstream raw materials:

2-(2-benzyloxy-acetylamino)-3-(4-methoxycarbonylmethoxy-phenyl)-propionic acid 2-methoxycarbonyl-ethyl ester

3-[4-(2-benzyloxy-acetoxy)-phenyl]-2-(2-benzyloxy-acetylamino)-propionic acid methoxycarbonylmethyl ester

2-(2-benzyloxy-acetylamino)-3-(4-hydroxy-phenyl)-propionic acid

2-(2-hydroxy-acetylamino)-3-(4-hydroxy-phenyl)-propionic acid methoxy carbonyl methyl ester

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