(E)-1,1-dimethyl-2-[(E)-2-methyl-4-(phenylthio)but-2-enylidene]hydrazine

Base Information

Chemical Name:(E)-1,1-dimethyl-2-[(E)-2-methyl-4-(phenylthio)but-2-enylidene]hydrazine
CAS No.:1606991-83-6
Molecular Formula:C₁₃H₁₈N₂S
Molecular Weight:234.365
Hs Code.:

Synonyms:(E)-1,1-dimethyl-2-[(E)-2-methyl-4-(phenylthio)but-2-enylidene]hydrazine

Suppliers and Price of (E)-1,1-dimethyl-2-[(E)-2-methyl-4-(phenylthio)but-2-enylidene]hydrazine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (E)-1,1-dimethyl-2-[(E)-2-methyl-4-(phenylthio)but-2-enylidene]hydrazine

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Technology Process of (E)-1,1-dimethyl-2-[(E)-2-methyl-4-(phenylthio)but-2-enylidene]hydrazine

There total 2 articles about (E)-1,1-dimethyl-2-[(E)-2-methyl-4-(phenylthio)but-2-enylidene]hydrazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

: 69690-06-8
4-formyl-3-methyl-2-butenyl phenyl sulfide

: 55484-54-3
N’,N’-dimethylhydrazine hydrochloride

: 1606991-83-6
(E)-1,1-dimethyl-2-[(E)-2-methyl-4-(phenylthio)but-2-enylidene]hydrazine

Guidance literature:: With triethylamine; In dichloromethane; at 20 ℃; for 1h; Inert atmosphere;

Reference yield: 63.0%

: 69690-06-8
4-formyl-3-methyl-2-butenyl phenyl sulfide

: 593-82-8,55484-54-3
N,N-dimethylhydrazine hydrochloride

: 1606991-83-6
(E)-1,1-dimethyl-2-[(E)-2-methyl-4-(phenylthio)but-2-enylidene]hydrazine

Guidance literature:: With triethylamine; In dichloromethane; at 20 ℃; for 24h; Inert atmosphere;
DOI:10.1021/jo500478u

Reference yield: 70.0%

: 1606991-83-6
(E)-1,1-dimethyl-2-[(E)-2-methyl-4-(phenylthio)but-2-enylidene]hydrazine

: 75-07-0,9002-91-9
acetaldehyde

: 1606991-73-4
(E)-3-[(E)-(2,2-dimethylhydrazono)methyl]-3-methyl-5-(phenylthio)pent-4-en-2-ol

Guidance literature:: (E)-1,1-dimethyl-2-[(E)-2-methyl-4-(phenylthio)but-2-enylidene]hydrazine; With sodium hexamethyldisilazane; In tetrahydrofuran; at -78 ℃; for 0.5h; Inert atmosphere;

acetaldehyde; In tetrahydrofuran; at -78 ℃; for 3.5h; Reagent/catalyst; Time; regioselective reaction; Inert atmosphere;
DOI:10.1021/jo500478u