1L-6-O-allyl-3,4,5-tri-O-benzyl-1-O-(4-methoxybenzoyl)-myo-inositol

Base Information

Chemical Name:1L-6-O-allyl-3,4,5-tri-O-benzyl-1-O-(4-methoxybenzoyl)-myo-inositol
CAS No.:154459-84-4
Molecular Formula:C₃₈H₄₂O₇
Molecular Weight:610.747
Hs Code.:

Synonyms:1L-6-O-allyl-3,4,5-tri-O-benzyl-1-O-(4-methoxybenzoyl)-myo-inositol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1L-6-O-allyl-3,4,5-tri-O-benzyl-1-O-(4-methoxybenzoyl)-myo-inositol

Chemical Property:

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Technology Process of 1L-6-O-allyl-3,4,5-tri-O-benzyl-1-O-(4-methoxybenzoyl)-myo-inositol

There total 9 articles about 1L-6-O-allyl-3,4,5-tri-O-benzyl-1-O-(4-methoxybenzoyl)-myo-inositol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 131233-71-1,1214020-75-3
1D-4-O-allyl-1,5,6-tri-O-benzyl-myo-inositol

: 824-94-2
p-methoxybenzyl chloride

: 154459-84-4
1L-6-O-allyl-3,4,5-tri-O-benzyl-1-O-(4-methoxybenzoyl)-myo-inositol

Guidance literature:: 1D-4-O-allyl-1,5,6-tri-O-benzyl-myo-inositol; With di(n-butyl)tin oxide; In methanol; for 2h; Inert atmosphere; Reflux;

p-methoxybenzyl chloride; With tetrabutylammomium bromide; In toluene; for 6h; Inert atmosphere; Molecular sieve; Reflux;
DOI:10.1016/j.tetlet.2011.06.005

Reference yield:

: 23393-20-6,111901-82-7,126722-28-9,134109-10-7,134109-11-8,136375-66-1,120202-94-0
D-1-O-benzyl-2,3:5,6-di-O-cyclohexylidene-myo-inositol

: 154459-84-4
1L-6-O-allyl-3,4,5-tri-O-benzyl-1-O-(4-methoxybenzoyl)-myo-inositol

Guidance literature:: Multi-step reaction with 5 steps

1.1: 100 percent / NaH / dimethylformamide / 0.75 h / 20 °C

2.1: 78 percent / pyridinium p-toluenesulfonate; p-toluenesulfonic acid / CH₂Cl₂; methanol / 1.17 h / 40 °C

3.1: 84 percent / sodium hydride / dimethylformamide / 4 h / 20 °C

4.1: 95 percent / camphor-10-sulfonic acid / CH₂Cl₂; methanol / 24 h / 20 °C

5.1: dibutyltin oxide / toluene / 3 h / Heating

5.2: 79 percent / tetrabutylammonium iodide / toluene / 1.5 h / 110 °C

With camphor-10-sulfonic acid; pyridinium p-toluenesulfonate; sodium hydride; di(n-butyl)tin oxide; toluene-4-sulfonic acid; In methanol; dichloromethane; N,N-dimethyl-formamide; toluene;
DOI:10.1016/j.carres.2003.06.002

Reference yield:

: 154459-83-3
1L-6-O-allyl-3-O-benzyl-1,2-O-cyclohexylidene-myo-inositol

: 154459-84-4
1L-6-O-allyl-3,4,5-tri-O-benzyl-1-O-(4-methoxybenzoyl)-myo-inositol

Guidance literature:: Multi-step reaction with 3 steps

1.1: 84 percent / sodium hydride / dimethylformamide / 4 h / 20 °C

2.1: 95 percent / camphor-10-sulfonic acid / CH₂Cl₂; methanol / 24 h / 20 °C

3.1: dibutyltin oxide / toluene / 3 h / Heating

3.2: 79 percent / tetrabutylammonium iodide / toluene / 1.5 h / 110 °C

With camphor-10-sulfonic acid; sodium hydride; di(n-butyl)tin oxide; In methanol; dichloromethane; N,N-dimethyl-formamide; toluene;
DOI:10.1016/j.carres.2003.06.002