6-azido-1',2,3,3',4,4'-hexa-O-benzyl-6'-O-(tert-butyldiphenylsilyl)-6-deoxysucrose

Base Information

• Chemical Name: 6-azido-1',2,3,3',4,4'-hexa-O-benzyl-6'-O-(tert-butyldiphenylsilyl)-6-deoxysucrose
• CAS No.: 1033507-62-8
• Molecular Formula: C₇₀H₇₅N₃O₁₀Si
• Molecular Weight: 1146.47
• Mol file: 1033507-62-8.mol

Synonyms:6-azido-1',2,3,3',4,4'-hexa-O-benzyl-6'-O-(tert-butyldiphenylsilyl)-6-deoxysucrose

Chemical Property of 6-azido-1',2,3,3',4,4'-hexa-O-benzyl-6'-O-(tert-butyldiphenylsilyl)-6-deoxysucrose

Chemical Property:

Purity/Quality:

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MSDS Files:

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Technology Process of 6-azido-1',2,3,3',4,4'-hexa-O-benzyl-6'-O-(tert-butyldiphenylsilyl)-6-deoxysucrose

There total 1 articles about 6-azido-1',2,3,3',4,4'-hexa-O-benzyl-6'-O-(tert-butyldiphenylsilyl)-6-deoxysucrose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

1',2,3,3',4,4'-hexa-O-benzyl-6'-O-(tert-butyldiphenylsilyl)-6-O-(methylsulfonyl)sucrose (1033507-59-3) → 6-azido-1',2,3,3',4,4'-hexa-O-benzyl-6'-O-(tert-butyldiphenylsilyl)-6-deoxysucrose (1033507-62-8)

Guidance literature:

With sodium azide; In N,N-dimethyl-formamide; at 90 ℃;

DOI:10.1055/s-2008-1032198

Reference yield: 99.0%

6-azido-1',2,3,3',4,4'-hexa-O-benzyl-6'-O-(tert-butyldiphenylsilyl)-6-deoxysucrose (1033507-62-8) → 6-azido-1',2,3,3',4,4'-hexa-O-benzyl-6-deoxysucrose (1033507-64-0)

Guidance literature:

With tetrabutyl ammonium fluoride; In tetrahydrofuran; for 3h; Heating;

DOI:10.1055/s-2008-1032198

upstream raw materials:

1',2,3,3',4,4'-hexa-O-benzyl-6'-O-(tert-butyldiphenylsilyl)-6-O-(methylsulfonyl)sucrose

Downstream raw materials:

6-azido-1',2,3,3',4,4'-hexa-O-benzyl-6-deoxysucrose