Diisopropyl-(2,4,6-tri-tert-butylphenylimino)silan

Base Information

• Chemical Name: Diisopropyl-(2,4,6-tri-tert-butylphenylimino)silan
• CAS No.: 102745-23-3
• Molecular Formula: C₂₄H₄₃NSi
• Molecular Weight: 373.698
• Mol file: 102745-23-3.mol

Synonyms:Diisopropyl-(2,4,6-tri-tert-butylphenylimino)silan

Chemical Property of Diisopropyl-(2,4,6-tri-tert-butylphenylimino)silan

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Diisopropyl-(2,4,6-tri-tert-butylphenylimino)silan

There total 4 articles about Diisopropyl-(2,4,6-tri-tert-butylphenylimino)silan which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

C24H43ClNSi(1-)*Li(1+) (102745-22-2) → Diisopropyl-(2,4,6-tri-tert-butylphenylimino)silan (102745-23-3)

Guidance literature:

at 80 ℃; under 0.008 Torr;

Reference yield:

difluorodiisopropylsilane (426-05-1) → Diisopropyl-(2,4,6-tri-tert-butylphenylimino)silan (102745-23-3)

Guidance literature:

Multi-step reaction with 3 steps

1: 90 percent / tetrahydrofuran; hexane / 2 h

2: 1) MeLi, 2) Me₃SiCl / 1) ether, 2) ether, THF, 1 h

3: 98 percent / 80 °C / 0.01 Torr

With chloro-trimethyl-silane; methyllithium; In tetrahydrofuran; hexane;

Reference yield:

2,4,6-tri-t-butylanilidolithium (102745-24-4) → Diisopropyl-(2,4,6-tri-tert-butylphenylimino)silan (102745-23-3)

Guidance literature:

Multi-step reaction with 3 steps

1: 90 percent / tetrahydrofuran; hexane / 2 h

2: 1) MeLi, 2) Me₃SiCl / 1) ether, 2) ether, THF, 1 h

3: 98 percent / 80 °C / 0.01 Torr

With chloro-trimethyl-silane; methyllithium; In tetrahydrofuran; hexane;

upstream raw materials:

C₂₄H₄₃ClNSi^(1-)*Li⁽¹⁺⁾

difluorodiisopropylsilane

2,4,6-tri-t-butylanilidolithium

(Fluoro-diisopropyl-silanyl)-(2,4,6-tri-tert-butyl-phenyl)-amine

Downstream raw materials:

2,2,4,4,6,6-hexaisopropylcyclotrisiloxane

[1-Phenyl-meth-(E)-ylidene]-(2,4,6-tri-tert-butyl-phenyl)-amine

Refernces