2-Methyl-2-(prop-2-en-1-yl)-1H-indene-1,3(2H)-dione

Base Information

Chemical Name:2-Methyl-2-(prop-2-en-1-yl)-1H-indene-1,3(2H)-dione
CAS No.:81055-91-6
Molecular Formula:C₁₃H₁₂O₂
Molecular Weight:200.237
Hs Code.:
DSSTox Substance ID:DTXSID20512312
Wikidata:Q82371499

Synonyms:81055-91-6;SCHEMBL8071793;2-Methyl-2-(prop-2-en-1-yl)-1H-indene-1,3(2H)-dione;DTXSID20512312

Suppliers and Price of 2-Methyl-2-(prop-2-en-1-yl)-1H-indene-1,3(2H)-dione

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of 2-Methyl-2-(prop-2-en-1-yl)-1H-indene-1,3(2H)-dione

Chemical Property:

Vapor Pressure:0.000291mmHg at 25°C
XLogP3:2.9
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:2
Exact Mass:200.083729621
Heavy Atom Count:15
Complexity:293

Purity/Quality:: 85.0-99.8% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CC1(C(=O)C2=CC=CC=C2C1=O)CC=C

Technology Process of 2-Methyl-2-(prop-2-en-1-yl)-1H-indene-1,3(2H)-dione

There total 2 articles about 2-Methyl-2-(prop-2-en-1-yl)-1H-indene-1,3(2H)-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 876-83-5
2-methyl-indan-1,3-dione

: 106-95-6
allyl bromide

: 81055-91-6
2-allyl-2-methyl-1,3-indandione

Guidance literature:: With celite coated with potassium fluoride; In acetonitrile; at 70 ℃; for 2h;

Reference yield:

: 81055-91-6
2-allyl-2-methyl-1,3-indandione

Guidance literature:: 2-Methyl-indandion-(1.3)-imin, Allylbromid u. Na-aethylat-Lsg. <Δ>;

Reference yield:

: 81055-91-6
2-allyl-2-methyl-1,3-indandione

: (2R,3S,3aR,8aS)-3-Benzoyl-2-ethyl-3a-hydroxy-8a-methyl-2,3,3a,8a-tetrahydro-1H-cyclopenta[a]inden-8-one

Guidance literature:: Multi-step reaction with 3 steps

1.1: O₃ / CH₂Cl₂ / -78 °C

1.2: triphenylphosphine / CH₂Cl₂ / 1 h / -78 - 20 °C

2.1: 1.32 g / CHCl₃ / 12 h / Heating

3.1: Cu(OTf)2; P(OEt)3 / CH₂Cl₂; hexane / 24 h / -20 °C

With copper(II) bis(trifluoromethanesulfonate); ozone; triethyl phosphite; In hexane; dichloromethane; chloroform; 2.1: Wittig olefination;
DOI:10.1021/ja030603l