Benzyl 2-(AcetylaMino)-3-O-[2-(acetylaMino)-2-deoxy-β-D-glucopyranosyl]-2-deoxy-α-D-galactopyranoside

Base Information

Chemical Name:Benzyl 2-(AcetylaMino)-3-O-[2-(acetylaMino)-2-deoxy-β-D-glucopyranosyl]-2-deoxy-α-D-galactopyranoside
CAS No.:85054-29-1
Molecular Formula:C₂₃H₃₄N₂O₁₁
Molecular Weight:514.53
Hs Code.:
Mol file:85054-29-1.mol

Synonyms:benzyl 2-acetamido-3-O-(2-acetamido-2-deoxy-β-D-glucopyranosyl)-2-deoxy-α-D-galactopyranoside

Suppliers and Price of Benzyl 2-(AcetylaMino)-3-O-[2-(acetylaMino)-2-deoxy-β-D-glucopyranosyl]-2-deoxy-α-D-galactopyranoside

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
Benzyl2-(Acetylamino)-3-O-[2-(acetylamino)-2-deoxy-β-D-glucopyranosyl]-2-deoxy-α-D-galactopyranoside
10mg
$ 1540.00

Medical Isotopes, Inc.
Benzyl2-(Acetylamino)-3-O-[2-(acetylamino)-2-deoxy-β-D-glucopyranosyl]-2-deoxy-α-D-galactopyranoside
1 mg
$ 675.00

Total 1 raw suppliers

Chemical Property of Benzyl 2-(AcetylaMino)-3-O-[2-(acetylaMino)-2-deoxy-β-D-glucopyranosyl]-2-deoxy-α-D-galactopyranoside

Chemical Property:

Solubility.:Methanol, Water

Purity/Quality:

95% ^*data from raw suppliers

Benzyl2-(Acetylamino)-3-O-[2-(acetylamino)-2-deoxy-β-D-glucopyranosyl]-2-deoxy-α-D-galactopyranoside ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Uses Oligosaccharide widely distributed in the human digestive tract.

Technology Process of Benzyl 2-(AcetylaMino)-3-O-[2-(acetylaMino)-2-deoxy-β-D-glucopyranosyl]-2-deoxy-α-D-galactopyranoside

There total 5 articles about Benzyl 2-(AcetylaMino)-3-O-[2-(acetylaMino)-2-deoxy-β-D-glucopyranosyl]-2-deoxy-α-D-galactopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.9%

: 85054-28-0
benzyl 2-acetamido-3-O-(2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-β-D-glucopyranosyl)-4,6-di-O-acetyl-2-deoxy-α-D-galactopyranoside

: 85054-29-1
benzyl 2-acetamido-3-O-(2-acetamido-2-deoxy-β-D-glucopyranosyl)-2-deoxy-α-D-galactopyranoside

Guidance literature:: With sodium methylate; In methanol; 1.) r.t., 2 h; 2.) in refrigerator, 2 h;
DOI:10.1016/0008-6215(83)88285-8

Reference yield:

: 117182-56-6
benzyl 2-acetamide-4,6-O-benzylidene-2-deoxy-α-D-galactopyranoside

: 85054-29-1
benzyl 2-acetamido-3-O-(2-acetamido-2-deoxy-β-D-glucopyranosyl)-2-deoxy-α-D-galactopyranoside

Guidance literature:: Multi-step reaction with 4 steps

1: 1.) silver trifluoromethanesulfonate, 2,4,6-trimethylpyridine, molecular sieves type 4A / 1.) dichloromethane, r.t., 1 h; 2.) dichloromethane, 4 h

2: 89.9 percent / 60 percent acetic acid / H₂O / 1.5 h / 85 °C

3: 1.) 85 percent hydrazine hydrate / 1.) ethanol, 70 deg C, 15 min; 2.) pyridine, 90 deg C, 20 min

4: 88.9 percent / 0.1 M sodium methoxide / methanol / 1.) r.t., 2 h; 2.) in refrigerator, 2 h

With 2,4,6-trimethyl-pyridine; 4 A molecular sieve; sodium methylate; silver trifluoromethanesulfonate; hydrazine hydrate; acetic acid; In methanol; water;
DOI:10.1016/0008-6215(83)88285-8

Reference yield:

: 85054-25-7
benzyl 2-acetamido-4,6-O-benzylidene-2-deoxy-3-O-(3,4,6-tri-O-acetyl-2-deoxy-2-phthalimido-β-D-glucopyranosyl)-α-D-galactopyranoside

: 85054-29-1
benzyl 2-acetamido-3-O-(2-acetamido-2-deoxy-β-D-glucopyranosyl)-2-deoxy-α-D-galactopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: 89.9 percent / 60 percent acetic acid / H₂O / 1.5 h / 85 °C

2: 1.) 85 percent hydrazine hydrate / 1.) ethanol, 70 deg C, 15 min; 2.) pyridine, 90 deg C, 20 min

3: 88.9 percent / 0.1 M sodium methoxide / methanol / 1.) r.t., 2 h; 2.) in refrigerator, 2 h

With sodium methylate; hydrazine hydrate; acetic acid; In methanol; water;
DOI:10.1016/0008-6215(83)88285-8