3,5-bis[3,5-bis(2,6-di-tert-butylpyridin-4-ylmethoxy)benzyloxy]benzyl alcohol

Base Information

Chemical Name:3,5-bis[3,5-bis(2,6-di-tert-butylpyridin-4-ylmethoxy)benzyloxy]benzyl alcohol
CAS No.:862009-39-0
Molecular Formula:C₇₇H₁₀₄N₄O₇
Molecular Weight:1197.7
Hs Code.:

Synonyms:3,5-bis[3,5-bis(2,6-di-tert-butylpyridin-4-ylmethoxy)benzyloxy]benzyl alcohol

Suppliers and Price of 3,5-bis[3,5-bis(2,6-di-tert-butylpyridin-4-ylmethoxy)benzyloxy]benzyl alcohol

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of 3,5-bis[3,5-bis(2,6-di-tert-butylpyridin-4-ylmethoxy)benzyloxy]benzyl alcohol

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 3,5-bis[3,5-bis(2,6-di-tert-butylpyridin-4-ylmethoxy)benzyloxy]benzyl alcohol

There total 3 articles about 3,5-bis[3,5-bis(2,6-di-tert-butylpyridin-4-ylmethoxy)benzyloxy]benzyl alcohol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 862009-38-9
3,5-bis(2,6-di-tert-butylpyridin-4-ylmethoxy)benzyl alcohol

: 862009-39-0
3,5-bis[3,5-bis(2,6-di-tert-butylpyridin-4-ylmethoxy)benzyloxy]benzyl alcohol

Guidance literature:: Multi-step reaction with 2 steps

1: 87 percent / PPh₃; CBr₄ / tetrahydrofuran / 0.5 h / 20 °C

2: 58 percent / K₂CO₃; 18-crown-6 / acetone / 168 h / Heating

With 18-crown-6 ether; carbon tetrabromide; potassium carbonate; triphenylphosphine; In tetrahydrofuran; acetone;
DOI:10.1055/s-2005-865355

Reference yield:

: 38222-83-2
2,6-di-tert-butyl-4-methylpyridine

: 862009-39-0
3,5-bis[3,5-bis(2,6-di-tert-butylpyridin-4-ylmethoxy)benzyloxy]benzyl alcohol

Guidance literature:: Multi-step reaction with 4 steps

1: 70 percent / NBS; AIBN / CCl₄ / 10 h / Heating

2: 77 percent / K₂CO₃; 18-crown-6 / acetone / 72 h / Heating

3: 87 percent / PPh₃; CBr₄ / tetrahydrofuran / 0.5 h / 20 °C

4: 58 percent / K₂CO₃; 18-crown-6 / acetone / 168 h / Heating

With N-Bromosuccinimide; 18-crown-6 ether; 2,2'-azobis(isobutyronitrile); carbon tetrabromide; potassium carbonate; triphenylphosphine; In tetrahydrofuran; tetrachloromethane; acetone;
DOI:10.1055/s-2005-865355

Reference yield:

: 81142-32-7
(2,6-di-tert-butyl-4-pyridyl)methylene bromide

: 862009-39-0
3,5-bis[3,5-bis(2,6-di-tert-butylpyridin-4-ylmethoxy)benzyloxy]benzyl alcohol

Guidance literature:: Multi-step reaction with 3 steps

1: 77 percent / K₂CO₃; 18-crown-6 / acetone / 72 h / Heating

2: 87 percent / PPh₃; CBr₄ / tetrahydrofuran / 0.5 h / 20 °C

3: 58 percent / K₂CO₃; 18-crown-6 / acetone / 168 h / Heating

With 18-crown-6 ether; carbon tetrabromide; potassium carbonate; triphenylphosphine; In tetrahydrofuran; acetone;
DOI:10.1055/s-2005-865355