9-hydroxy-10-phenyl-9,10-disilatriptycene

Base Information

Chemical Name:9-hydroxy-10-phenyl-9,10-disilatriptycene
CAS No.:1428127-16-5
Molecular Formula:C₂₄H₁₈OSi₂
Molecular Weight:378.577
Hs Code.:

Synonyms:9-hydroxy-10-phenyl-9,10-disilatriptycene

Suppliers and Price of 9-hydroxy-10-phenyl-9,10-disilatriptycene

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 9-hydroxy-10-phenyl-9,10-disilatriptycene

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Technology Process of 9-hydroxy-10-phenyl-9,10-disilatriptycene

There total 2 articles about 9-hydroxy-10-phenyl-9,10-disilatriptycene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 1395949-98-0
9-phenyl-9,10-disilatriptycene

: 1428127-16-5
9-hydroxy-10-phenyl-9,10-disilatriptycene

Guidance literature:: With water; sodium hydroxide; In tetrahydrofuran; at 20 ℃; for 1h; Inert atmosphere;
DOI:10.1021/om301170r

Reference yield:

: 583-53-9
2,3-dibromobenzene

: 1428127-16-5
9-hydroxy-10-phenyl-9,10-disilatriptycene

Guidance literature:: Multi-step reaction with 3 steps

1.1: n-butyllithium / diethyl ether; tetrahydrofuran; hexane / 1 h / -110 °C / Inert atmosphere

1.2: 0.5 h / -110 - 20 °C / Inert atmosphere

1.3: 1 h / 0 °C / Inert atmosphere

2.1: magnesium / tetrahydrofuran / 1 h / 100 °C / Inert atmosphere; Sealed tube

2.2: 1 h / 180 °C / Inert atmosphere; Sealed tube; Microwave irradiation

2.3: Inert atmosphere

3.1: sodium hydroxide; water / tetrahydrofuran / 1 h / 20 °C / Inert atmosphere

With n-butyllithium; water; magnesium; sodium hydroxide; In tetrahydrofuran; diethyl ether; hexane;
DOI:10.1021/om301170r