1,3-diphenyl-7-(4-methoxyphenyl)-5-p-tolyl-1,6,7,8-tetrahydropyrazolo[4,3-b][1,4]diazepine

Base Information

Chemical Name:1,3-diphenyl-7-(4-methoxyphenyl)-5-p-tolyl-1,6,7,8-tetrahydropyrazolo[4,3-b][1,4]diazepine
CAS No.:1338328-66-7
Molecular Formula:C₃₂H₂₈N₄O
Molecular Weight:484.601
Hs Code.:

Synonyms:1,3-diphenyl-7-(4-methoxyphenyl)-5-p-tolyl-1,6,7,8-tetrahydropyrazolo[4,3-b][1,4]diazepine

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Chemical Property of 1,3-diphenyl-7-(4-methoxyphenyl)-5-p-tolyl-1,6,7,8-tetrahydropyrazolo[4,3-b][1,4]diazepine

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Technology Process of 1,3-diphenyl-7-(4-methoxyphenyl)-5-p-tolyl-1,6,7,8-tetrahydropyrazolo[4,3-b][1,4]diazepine

There total 4 articles about 1,3-diphenyl-7-(4-methoxyphenyl)-5-p-tolyl-1,6,7,8-tetrahydropyrazolo[4,3-b][1,4]diazepine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 122128-84-1
1,3-diphenyl-1H-pyrazole-4,5-diamine

: 6552-66-5,50990-40-4,102692-51-3
3-(4-methoxyphenyl)-1-p-tolylprop-2-en-1-one

: 1338328-66-7
1,3-diphenyl-7-(4-methoxyphenyl)-5-p-tolyl-1,6,7,8-tetrahydropyrazolo[4,3-b][1,4]diazepine

Guidance literature:: In ethanol; at 160 ℃; for 0.25h; Microwave irradiation;
DOI:10.1002/cjoc.201180265

Reference yield:

: 5356-71-8
1,3-diphenyl-1H-pyrazol-5-amine

: 1338328-66-7
1,3-diphenyl-7-(4-methoxyphenyl)-5-p-tolyl-1,6,7,8-tetrahydropyrazolo[4,3-b][1,4]diazepine

Guidance literature:: Multi-step reaction with 3 steps

1: hydrogenchloride; sodium nitrite / water / 0 - 20 °C

2: hydrogenchloride; tin(ll) chloride / water / 0.25 h / 0 - 20 °C

3: ethanol / 0.25 h / 160 °C / Microwave irradiation

With hydrogenchloride; tin(ll) chloride; sodium nitrite; In ethanol; water; 3: Michael condensation;
DOI:10.1002/cjoc.201180265

Reference yield:

: 90012-56-9
4-nitroso-1,3-diphenyl-1H-pyrazol-5-amine

: 1338328-66-7
1,3-diphenyl-7-(4-methoxyphenyl)-5-p-tolyl-1,6,7,8-tetrahydropyrazolo[4,3-b][1,4]diazepine

Guidance literature:: Multi-step reaction with 2 steps

1: hydrogenchloride; tin(ll) chloride / water / 0.25 h / 0 - 20 °C

2: ethanol / 0.25 h / 160 °C / Microwave irradiation

With hydrogenchloride; tin(ll) chloride; In ethanol; water; 2: Michael condensation;
DOI:10.1002/cjoc.201180265